Preparation method of diamond wire and prepared diamond wire
A diamond wire and diamond particle technology, applied in metal material coating process, coating and other directions, can solve the problems of low strength of diamond wire, easy to break, easy to fall off of diamond particles, etc. shedding effect
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Embodiment 1
[0034] Step 1: Diamond and Metal Powder Mixing
[0035] Diamonds with a particle size of 9-15 μm are degreased through 10% Na(OH) aqueous solution, rinsed with water, and then pickled with 5% aqua regia to remove impurities on the surface of the diamond. Tin powder with an average particle size of 12 μm, lead powder with an average particle size of 8 μm and copper powder with an average particle size of 25 μm are mixed in a weight ratio of diamond: tin: lead: copper=1:4:5:1.5. The mixed powder is placed in a mixer equipped with an alcohol dispersant and mixed and ball-milled at a ball-to-material ratio of 5:1, and the ball-milling medium used is cemented carbide with a particle size of 3 mm. A powder mixture is obtained.
[0036] Step 2: Heating the mixed powder with an induction coil
[0037] Take the mixed powder obtained in the first step and put it into a crucible, then place the crucible in a container equipped with an induction heating device, and heat the mixed powder...
Embodiment 2
[0043] Step 1: Diamond and Metal Powder Mixing
[0044] Take diamond powder with a particle size range of 35-70 μm, degrease through 10% Na(OH) aqueous solution, rinse with water, and then pickle with 5% aqua regia to remove impurities on the diamond surface. Tin powder with an average particle size of 4 μm, lead powder with an average particle size of 5 μm and copper powder with an average particle size of 6 μm are mixed in a weight ratio of diamond: tin: lead: copper=1.1:5:6.5:2. The mixed powder was placed in a mixer equipped with a dispersant SPS and mixed and ball-milled at a ball-to-material ratio of 4:1, and the ball-milling medium used was stainless steel balls with a particle size of 10 mm. A powder mixture is obtained.
[0045] Step 2: Resistance wire heating mixed powder
[0046] Put the mixed powder obtained in the first step into a crucible, then place the crucible in a container equipped with a resistance wire heating device, and heat the mixed powder to 330°C ...
Embodiment 3
[0051] Step 1: Diamond and Metal Powder Mixing
[0052] Take diamond powder with a particle size distribution range of 70-100 μm, degrease through 10% Na(OH) aqueous solution, rinse with water, and then pickle with 5% aqua regia to remove impurities on the diamond surface. Tin powder with an average particle size of 8 μm, lead powder with an average particle size of 9 μm and copper powder with an average particle size of 3 μm are mixed in a weight ratio of diamond: tin: lead: copper=1.2:6.5:8:2.5. The mixed powder is placed in a mixer and mixed and ball-milled at a ball-to-material ratio of 3:1 to obtain a powder mixture;
[0053] Step 2: Induction Heating Mixed Powder
[0054] Put the mixed powder obtained in the first step into a crucible, then place the crucible in a container equipped with an induction heating device, and heat the mixed powder to 350°C to obtain an alloy melt containing diamond particles;
[0055] The third step: diamond particle alloy melt cladding
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