Rapid reducing method of catalyst
A catalyst and fast technology, applied in chemical instruments and methods, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve the problems of large hydrogen consumption, long catalyst reduction time, etc., achieve short reduction time, save hydrogen, time-saving effect
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[0026] The method of the present invention is applied to the nickel-based catalyst reduction process. The loading amount of nickel-based catalyst is 1.0m 3 , the heating rate is 10℃ / h, and the gas flow rate at the inlet of the reduction furnace is 500m 3 / h, the hydrogen concentration is 75%, and the specific steps of the traditional reduction method and the method of the present invention are shown in Table 1. The reduced catalyst is at 152°C and the volume space velocity of acetone is 0.5h -1 , Acetone: hydrogen: the mol ratio of ammonia is 1: 3: 3, and the evaluation result on the isopropylamine evaluation device that catalyst consumption is 50ml is shown in Table 2.
[0027] The specific operation of the method of the present invention is as follows: the heating rate of the reduction furnace is set to be 10° C. / h, and the inlet gas flow rate is 500 m 3 / h, the hydrogen concentration is 75%, turn on the reduction control program to increase the temperature, and analyze t...
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