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Application of silica nano material in polyester-imide enameled wire insulating varnish

A technology of enameled wire insulation and silicon dioxide, applied in the direction of coating, etc., can solve the problems of easy gelation of insulating varnish, complex process, rough surface of enameled wire, etc., and achieve the effect of stable process production and wide process margin

Inactive Publication Date: 2012-01-18
上海晟然绝缘材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This is very effective for nano-materials such as titanium dioxide and aluminum oxide. Since silica nano-materials are easy to agglomerate, it is difficult to disperse silica to insulating varnishes with an average particle size of less than 100 nanometers by the above method, resulting in the enameled wire during use. Matte surface with bright spots
It is also reported abroad that the sol-gel method is used to prepare silica nano-polyesterimide enameled wire insulating varnish, but the process is complicated, domestic enterprises have not mastered the key technology, and the insulating varnish made is easy to gel during storage and cannot be used.

Method used

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  • Application of silica nano material in polyester-imide enameled wire insulating varnish

Examples

Experimental program
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Effect test

Embodiment 1

[0021] With 6 parts of silicon dioxide nanomaterials (particle diameter 25 nanometers), adopt the method of the present invention, disperse in 50 parts of polyesterimide paints, 50 parts of modified polyester paints, and use this as primer, polyamide imide The amine enameled wire insulation varnish is used as the top coat (such as Shanghai Shengran's 338 / 35), and it is made into a 200-grade polyamide-imide composite polyesterimide frequency conversion enameled wire.

[0022] The method for dispersing silica nanomaterials in polyesterimide paint is as follows:

[0023] (1) Pre-disperse 6 parts of nano-silica and 0.6 parts of γ-aminopropyltriethoxysilane (KH550) in 40 parts of modified polyester paint, and feed the silica in 9 times In dispersion A, each interval is 30 minutes to generate pre-dispersion A;

[0024] (2) Add 50 parts of polyesterimide enameled wire insulating varnish and 10 parts of modified polyester varnish to pre-dispersion A, and disperse for 1 hour to form p...

Embodiment 2

[0027] With 8 parts of silicon dioxide nanomaterials (particle diameter 25 nanometers), adopt embodiment 1 method, disperse in 50 parts of polyesterimide paints, in 50 parts of modified polyester paints, and use this as primer, polyamide amide The insulating varnish of imide enameled wire is the top coat (such as Shanghai Shengran's 338 / 35), which is made into 200-grade polyamide-imide composite polyesterimide frequency conversion enameled wire.

[0028] Preparation of enameled wire sample wire

[0029] Coating process parameters are as follows:

[0030] Coating equipment: Meda QHLF1 / 2

[0031] Process parameters:

[0032] Oven inlet: 230°C; Lower layer of oven: 350°C; Supplementary heating after catalysis: 520°C; Circulation fan: 2100RPM; Exhaust fan: 800RPM; Cooling fan: 400RPM

[0033] Speed: 30 m / min

[0034] Painting passes: 9+3

[0035] The enameled wire specification is 1.05

[0036]

[0037] The test method of corona resistance life is: rise time 200 nanosecon...

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PUM

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Abstract

The invention relates to an application of a silica nano material in polyester-imide enameled wire insulating varnish. The method for dispersing nano-silica in polyester-imide varnish comprises the following steps in sequence: predispersing 6-8 parts of nano-silica and 0.6 parts of gamma-aminopropyl triethoxysilane (KH550) in 40 parts of modified polyester varnish, feeding silica into the above pre-dispersion A for not less than three times at intervals of 20-40 min so as to generate a pre-dispersion A; adding 50 parts of polyester-imide enameled wire insulating varnish and 10 parts of modified polyester enameled wire insulating varnish into the pre-dispersion A, dispersing for 1 hour to generate a pre-dispersion B; performing circulating continuous dispersion of the pre-dispersion B in a rod-pin dispenser for 3 hours, wherein the temperature of a dispersing cavity is controlled to be not more than 70 DEG C. Enameled wires prepared by the method of the invention have corona resistance which is up to above 100 times of that of common enameled wires; the prepared enameled wires have smooth surfaces without bright spots; the storage life of the insulating varnish is up to 1 year; the process has wide redundancy, and is convenient for the realization of robust process production.

Description

technical field [0001] The invention discloses a silicon dioxide nanometer material used in polyesterimide enameled wire insulating varnish, and relates to a dispersion technology in which silicon dioxide nanometer material is dispersed in polyesterimide enameled wire insulating varnish. Background technique [0002] When IGBT frequency conversion stepless speed regulation, a towering sharp wave rising instantaneously will be generated in the electromagnetic coil, and corona will be generated on the electromagnetic wire, and the insulation structure of the electromagnetic wire will be electrically aged under the action of the corona, causing the insulation structure to be damaged prematurely. . The solution is generally to add materials such as nano-silica, nano-titanium dioxide, and nano-alumina to the insulating paint. The dispersion of nano-materials in the paint is the key core technology. At present, paint manufacturers at home and abroad generally use the disc dispers...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D179/08C09D7/12C09D5/25
Inventor 邵武军涂张应
Owner 上海晟然绝缘材料有限公司
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