Device for analyzing gas phase chemical components of cigarette smoke on line
A gas-phase chemistry and analysis device technology, which is applied to measurement devices, analysis materials, material analysis by electromagnetic means, etc., can solve the problem that the residual interference effect of smoke cannot be eliminated well, and continuous automatic detection of cigarette smoke cannot be performed. Flue gas analysis results comparison and other issues, to achieve good qualitative and quantitative analysis results, simple structure, and reduce the effect of interference effects
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Embodiment 1
[0046] Smoking cigarettes under standard smoking conditions, that is, 35ml per puff, puffing for 2 seconds, with a puffing gap of 58 seconds. Before the cigarette is smoked, the volume in the pipe from the smoke introduction two-way valve 12 to the smoke introduction and outlet 4 is constant and in a vacuum state, so when setting the suction volume of the smoking machine, this The volume in part of the pipe should be considered, that is, the actual suction volume of the smoking machine should be 35ml minus the volume in the pipe; the online analysis mass spectrometer uses synchrotron radiation as the ionization light source, and the photon energy is selected as 11.0eV. Scan the flue gas immediately after inhaling, and set the scan time of each flue gas to 10 seconds, that is to say, you can obtain a single-puff flue gas mass spectrum during puff-by-puff analysis. Refer to the analysis results Figure 4 .
[0047] In addition, in order to verify the effect of the present invention...
Embodiment 2
[0049] The smoking conditions of the smoking machine were the same as in Example 1, and the photon energy of the synchrotron radiation photoionization online analysis mass spectrometer was selected to be 12.0 eV. After the first puff of smoke is finished, turn off the smoking machine and other working accessories. At the same time, immediately start the online analysis mass spectrometer to scan and test at regular intervals. Each scan time is 5 seconds. The total analysis The time is 240 seconds, and the change rule of the component to be measured can be obtained.
[0050] Image 6 The changes over time of several representative flue gas components with mass numbers of 32, 60 and 61 are given.
[0051] Therefore, the cigarette smoke gas phase chemical composition online analysis device provided by the present invention effectively eliminates the influence of the upper puff smoke on the lower puff gas composition analysis result when the cigarette is smoked puff by puff, and can be...
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