Modified pearl cherry vitamin C sleeping mask and preparation method thereof
A sleep mask, modified technology, applied in the field of modified pearl cherry vitamin C sleep mask and its preparation, can solve the problems of easy aggregation of nano-pearl powder, hydrophilic and oleophobic, etc., achieve affinity enhancement, repair fatigue and dryness Thirst, good permeability effect
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Embodiment 1
[0058] Step 1, carry out modified treatment to pearl powder according to the following methods:
[0059] The mass fraction is 20% pearl powder (average particle diameter 50 nanometers) suspoemulsion is added in the reactor, is heated to activation temperature and is 85 ℃, adds and accounts for the tensio-active agent of 2% of pearl powder dry weight, constantly stirs 20min, then with 3500 Centrifuge at rpm for 10 minutes and collect modified pearl powder, dry and pulverize to obtain modified pearl powder. Wherein the surfactant used is composed of (w%) 45% Span 80, 25% polyethylene glycol 400 and 30% butyl acetate, and the pearl powder is coated with the active agent.
[0060] Step 2, take raw materials according to the following ratio:
[0061] Glyceryl polyether-26 10kg Modified pearl powder 0.1kg
[0062] Butanediol 5kg Ascorbyl Glucoside 0.1kg
[0063] Isononyl isononanoate 3kg Preservative 1kg
[0064] Cetearyl Alcohol 2kg Polyquaternium-51 0.5kg
[0065] Tween 20 1k...
Embodiment 2
[0076] Step 1: Carry out modification treatment to pearl powder according to the following method:
[0077] The pre-prepared mass fraction of 15% pearl powder (average particle diameter at 100 nanometers) suspoemulsion is added to the reactor, heated at a constant temperature, and the activation temperature is 75 ° C, adding the prepared surface active agent that accounts for 1.5% of the dry weight of pearl powder. The mixture was continuously stirred for 40 minutes, then centrifuged at 3000 rpm for 20 minutes, dried at a constant temperature, and crushed by air flow to obtain modified nano-pearl powder. Wherein the surfactant used is composed of (w%) 60% Span 80, 20% polyethylene glycol 400 and 20% butyl acetate, and the pearl powder is coated with the active agent.
[0078] Step 2: Weigh the raw materials according to the following proportions:
[0079] Glyceryl polyether-26 6kg Modified pearl powder 0.8kg
[0080] Butanediol 8kg Ascorbyl Glucoside 0.5kg
[0081] Isononyl...
Embodiment 3
[0094] Step 1: Carry out modification treatment to pearl powder according to the following method:
[0095] The pre-prepared mass fraction of 30% pearl powder (average particle size is 150 nanometers) suspoemulsion is added in the reactor, heated at a constant temperature, the activation temperature is 80 ° C, and the surfactant that is prepared and accounts for 2.5% of the dry weight of pearl powder is added , continuously stirred for 30 minutes, then centrifuged at 3000 rpm for 15 minutes, dried at a constant temperature, and crushed by air flow to obtain modified nano pearl powder. Wherein the surfactant used is composed of (w%) 50% Span 80, 30% polyethylene glycol 400 and 20% butyl acetate, and the pearl powder is coated with the active agent.
[0096] Step 2: Weigh the raw materials according to the following proportions:
[0097] Glyceryl polyether-26 8kg Modified pearl powder 0.8kg
[0098] Butanediol 8kg Ascorbyl Glucoside 0.5kg
[0099] Isononyl isononanoate 1kg Pr...
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