Method for synthesizing porous BiFeO3 nano microcrystal by using P123 assisting sol gel process
A sol-gel method, P123 technology, applied in the direction of nanotechnology, nanotechnology, nanostructure manufacturing, etc., can solve the problems of inadaptability to the concept of green conservation and environmental protection, grain growth, impurity, low efficiency, etc.
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[0018] Embodiment: the preparation process and steps in the present embodiment are as follows:
[0019] (1) Preparation of raw materials: Weigh 4.0400g of analytically pure Fe (NO 3 ) 3 9H 2 O and 4.8507g of analytically pure Bi(NO 3 ) 3 ·5H 2 O is used as a raw material, the two are mixed and placed in a 150ml round bottom flask;
[0020] (2) Preparation of sol: Add 20ml of analytically pure ethylene glycol into the above-mentioned flask as a solvent and a complexing agent, and through magnetic stirring, completely dissolve the inorganic salt raw material to become a uniform mixed solution; add 1ml of analytically pure glacial acetic acid as a stabilizer , put the above solution in an oil bath device, and stir at a constant temperature of 70°C for 30 minutes. At this time, a condensation reflux device should be added to prevent the solution from evaporating too quickly; Stir at constant temperature for 2 hours at ℃ to obtain a maroon sol;
[0021] (3) Formation of gel:...
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