High-efficiency extraction agent and method for extracting H acid waste liquid
An extraction agent and extraction technology, applied in chemical instruments and methods, extraction water/sewage treatment, natural water treatment, etc., can solve the problems of long H acid production process, high COD in wastewater, and difficult biodegradation, and improve production conversion. efficiency, simple equipment, and easy availability of raw materials
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[0018] 1. Preparation of extractant:
[0019] Equipment: mixing tank, 500L jacket with stirring, liquid pump, storage tank.
[0020] First take the required raw materials: 130.4Kg of tertiary dodecylamine, 304.3Kg of sulfonated kerosene and 65.2Kg of tributyl phosphate.
[0021] Weigh the above-mentioned materials and pour them into their respective high-level tanks, first add sulfonated kerosene into the mixing tank in order to start stirring, the jacket is heated to 50°C, and then dropwise add dodecyl tertiary amine and phosphoric acid from the high-level tanks Stir for 90 minutes after all the tributyl esters have been added and take a sample for analysis (the content of each component is detected by gas chromatography), after passing the test, leave it to stand down to room temperature, and put it into a storage tank for subsequent use.
[0022] 2. Take H acid production waste liquid pH 1.0, temperature 55°C, press 0.3m 3 At the same time, the extraction agent and H acid...
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