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Super-pure smelting method for industrially producing Incone1690 alloy

An alloy and pure technology, applied in the field of vacuum induction melting, can solve the problems of low alloy thermal processing yield, inability to alloy thermal processing, low high-temperature plasticity of alloys, etc., and achieve the effects of improving high-temperature plasticity, improving thermal processing performance, and improving purity

Active Publication Date: 2010-02-10
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Usually, MgO or MgO-Al is used in industrial vacuum induction melting to produce Inconel690 alloy. 2 o 3 The crucible made of refractory material cannot achieve high-temperature deoxidation and desulfurization during the refining period, and no strong deoxidation and desulfurization agents are added at the end of the smelting period.
Generally, the oxygen and sulfur content of the alloy produced is about 20ppm.wt (weight), which cannot reach ultra-pure
Therefore, the high temperature plasticity of the alloy is low, and the ideal hot working of the alloy cannot be carried out, so that the hot working yield of the alloy is low

Method used

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  • Super-pure smelting method for industrially producing Incone1690 alloy

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Embodiment 1

[0022] A crucible knotted with high-purity, thermodynamically stable CaO refractory material is used to melt the I-690 alloy for industrial production. The melting process includes: charging → melting period → refining period → condensation → deoxidation and desulfurization period → pouring; among them, charging , melting period, and pouring are conventional techniques. The specific process is:

[0023] (1) The crucible for smelting is a 500kg crucible knotted with CaO, and the purity of CaO is ≥98.5wt%;

[0024] (2) Alloy raw materials: According to the composition requirements, take Ni plate, pure Fe, metal Cr, C and other alloy elements, deoxidizer and desulfurizer.

[0025] In this step, the deoxidizer is a Ni-Ca master alloy: Ni 80wt%, Ca 20wt%; or, the deoxidizer is a Ni-Mg master alloy: Ni 80wt%, Mg 20wt%; the desulfurizer is a Ni-Ca master alloy: Ni 80wt%, Ca 20wt%.

[0026] (3) Alloy charging: put the main raw materials Ni, Cr, C, and Fe into the crucible, and put ...

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Abstract

The invention belongs to the technical field of vacuum induction smelting, and relates to an improvement on a smelting process for industrially producing Incone1690 alloy, in particular to a super-pure smelting process for industrially producing Incone1690 alloy. The process uses a CaO fireproof material with high purity (CaO is more than 98.5 percent) and good thermodynamic stability as a crucible material for the vacuum induction smelting. The specific smelting process comprises charging, smelting period, refining period, condensing, deoxidizing and desulfurizing period and casting, whereinin the refining period, effective deoxidization and desulfurization are carried out on the wall part of a crucible and the surface of molten steel by improving the refining temperature and strengthening the thermodynamic and kinetic conditions of deoxidization and desulfurization; and in the deoxidizing and desulfurizing period, final deoxidization and desulfurization are carried out for the alloyby adding strong deoxidizing and desulfurizing agent so as to further reduce the contents of oxygen and sulfur in the alloy below 10 ppm.wt. The process effectively improves the high-temperature plasticity of the alloy, improves the thermal processing performance of the alloy, and obtains the high-quality alloy.

Description

technical field [0001] The invention relates to the field of vacuum induction smelting, in particular to an ultra-pure smelting process for industrial production of I-690 alloy. Background technique [0002] Inconel690 alloy is an American brand, and its main components range as follows: [0003] [0004] Usually, MgO or MgO-Al is used in industrial vacuum induction melting to produce Inconel690 alloy. 2 o 3 The crucible made of refractory material cannot achieve high-temperature deoxidation and desulfurization during the refining period, and no strong deoxidizing and desulfurizing agents are added at the end of the smelting period. Generally, the oxygen and sulfur content of the alloy produced is about 20ppm.wt (weight), which cannot be ultra-pure. Therefore, the high-temperature plasticity of the alloy is low, and the alloy cannot be ideally hot-worked, resulting in a low yield of hot-worked alloys. Contents of the invention [0005] The purpose of the present inv...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C33/04C21C7/04
Inventor 高明刘奎马颖澈万柏方张建国张顺南李依依
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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