Hydraulic structure disjoint filling silicone adhesive and preparation method thereof
A technology of hydraulic structure and silicone glue, applied in chemical instruments and methods, adhesives, other chemical processes, etc., can solve the problems of unable to form gel, unable to meet the requirements of elastic cushion, low sampling success rate, etc.
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Embodiment 1
[0017] The hollow filling silicone glue for the hydraulic structure of the present invention is made of the following two-components A and B) at a weight ratio of 7.9:1: wherein component A is prepared from the following raw materials in the weight ratio:
[0018] α,ω-Dihydroxypolydimethylsiloxane 100
[0019] Calcium carbonate filler 37
[0020] Component B is prepared from the following raw materials in weight ratio:
[0021] Calcium Carbonate Filler 4
[0022] Methylvinyldisilane 10
[0023] Linear aminooxy-containing polysiloxane crosslinkers 3.3.
[0024] Preparation method: α, ω-dihydroxy polydimethylsiloxane and calcium carbonate filler in component A are mixed in a three-arm planetary mixer at a weight ratio of 100:37, and then sealed for later use; calcium carbonate in component B Filler, methyl vinyl disilane and linear aminooxy-containing polysiloxane crosslinking agent are mixed in a three-arm planetary mixer in a weight ratio of 4:10:3.3, and then sealed for u...
Embodiment 2
[0026] The hydraulic structure of the present invention is void-filled silicone glue, which is made of the following two components of A and B in a weight ratio of 8:1:
[0027] Among them, component A is prepared from the following raw materials in weight ratio:
[0028] α,ω-Dihydroxypolydimethylsiloxane 100
[0029] Calcium carbonate filler 30
[0030] Component B is prepared from the following raw materials in weight ratio:
[0031] Calcium Carbonate Filler 3
[0032] Methylvinyldisilane 10
[0033] Linear aminooxy-containing polysiloxane crosslinkers 3.3.
[0034] Preparation method: α, ω-dihydroxy polydimethylsiloxane and calcium carbonate filler in component A are mixed in a three-arm planetary mixer at a weight ratio of 100:30, and then sealed for later use; calcium carbonate in component B Filler, methyl vinyl disilane and linear aminooxy-containing polysiloxane crosslinking agent are mixed in a three-arm planetary mixer in a weight ratio of 3:10:3.3, and then sea...
Embodiment 3
[0036] The hydraulic structure of the present invention is void-filled silicone glue, which is made of the following two components of A and B in a weight ratio of 6.6:1:
[0037] Among them, component A is prepared from the following raw materials in weight ratio:
[0038] α,ω-Dihydroxypolydimethylsiloxane 100
[0039] Calcium carbonate filler 30
[0040] Component B is prepared from the following raw materials in weight ratio:
[0041] Calcium Carbonate Filler 3
[0042] Methylvinyldisilane 10
[0043] Linear aminooxy-containing polysiloxane crosslinkers 6.7.
[0044] Preparation method: α, ω-dihydroxy polydimethylsiloxane and calcium carbonate filler in component A are mixed in a three-arm planetary mixer at a weight ratio of 100:30, and then sealed for later use; calcium carbonate in component B Filler, methyl vinyl disilane and linear aminooxy-containing polysiloxane crosslinking agent are mixed in a three-arm planetary mixer in a weight ratio of 3:10:6.7, and then s...
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