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Pollution-free production technology of direct fast black G

A production process, non-polluting technology, applied in the direction of polyazo dyes, etc., can solve the problems of increasing product cost, environmental pollution, etc., and achieve the effect of reducing the difficulty of treatment

Active Publication Date: 2009-11-18
INNER MONGOLIA XINYA CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, a large amount of waste water is produced in the traditional production process of the dye, which will cause serious environmental pollution if discharged without treatment
And the treatment of process wastewater will increase the cost of the product

Method used

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  • Pollution-free production technology of direct fast black G
  • Pollution-free production technology of direct fast black G
  • Pollution-free production technology of direct fast black G

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Embodiment Construction

[0030] Below in conjunction with accompanying drawing and preferred embodiment, the specific implementation mode that provides according to the present invention is described in detail as follows:

[0031] like figure 2 Shown, a kind of pollution-free production technology of direct sunfast black G is characterized in that the implementation steps are as follows:

[0032] (1) Diazotization of p-nitroaniline:

[0033] Drain 50-55ml of water, add 13g of p-nitroaniline and 28g of 30% hydrochloric acid, stir for 2 hours, add ice cubes and cool down to t=0-5°C; quickly add 3.7g of sodium nitrite, and then spend 10-30 minutes on the liquid surface Then add 3.7g of sodium nitrite; after the addition, the temperature t=5~10°C, and it is detected as blue with Congo red test paper and starch potassium iodide test paper; continue to stir for 2~2.5 hours until all p-nitroaniline is dissolved as the reaction end point, Then add sulfamic acid to neutralize excess nitrous acid;

[0034] ...

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Abstract

The invention relates to a pollution-free production technology of direct fast black G, comprising the following implementation steps: firstly, primary acid coupling is carried out on nitroaniline after diazotization and H-acid; after the full reaction of the H-acid is detected, sodium carbonate is added and pH is adjusted to 8 to 8.2 to carry out secondary basic coupling; the coupling product is added into a sodium sulfide solution for reduction, and the temperature gradually raises to t of 38 DEG C to 40 DEG C in the reaction process; after the sodium carbonate is added into the reduction product after acidification to adjust the pH of a medium to 7.5 to 8, the mixture is adsorbed by activated carbon and filtered, and ternary coupling is carried out on the obtained filter liquor after diazotization and lentine; and after the reaction is detected to be end point, the materials are directly delivered to a drying tower for spray drying. In the invention, the reduced reaction solution does not need the processes of salting out, acidification and filtration, activated carbon adsorption is adopted instead. In the process, no waste liquor is generated, and environment pollution caused in the production process of dye is greatly reduced. Simultaneously, wastewater processing is not needed, and the cost is saved. The optimized technology directly transfers the reaction solution after ternary coupling into the drying tower for spray drying; and the yield and the coloring intensity of the dye are effectively increased, energy is saved, the consumption is reduced, and the effect is obvious.

Description

technical field [0001] The invention relates to a production process of a dye, in particular to a pollution-free production process of direct sunfast black G. Background technique [0002] At present, the competition in the direct dye industry is becoming increasingly fierce, and people's requirements for the color of textiles are also increasing, and the requirements for dyes are also getting higher and higher. Environmentally friendly dyes and salt-free liquid dyes with bright colors and high dye uptake are very popular. [0003] In the traditional production process of direct dyes, the process of salting out, filtration and concentration is generally carried out; the purpose is to desalt, remove unreacted raw materials, intermediates and secondary dyes, and remove water to obtain dyes with the required concentration and purity. It is then dried in an oven to make powdered dyes or directly prepared as liquid dyes. Practice has proved that the impurities and salt brought i...

Claims

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Application Information

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IPC IPC(8): C09B31/30
Inventor 张超水张宝文李新勇王淑娜李国栋
Owner INNER MONGOLIA XINYA CHEM
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