Preparation method of additive agent capable of causing flue-cured tobacco to have fragrance of oolong tea, flavoring as well as application in flue-cured tobacco
A technology for oolong tea and additives, which is used in the preparation of tobacco, essential oils/spice, and applications, can solve problems such as increased irritation, increased tar content, and mixed smoke, and achieves reduced irritation, reduced harm, and taste. the effect of coordination
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[0029] One, the preparation method of additive for oolong tea cigarette:
[0030] Following each embodiment is all with total amount being 100 grams, as the basis of test.
Embodiment 1
[0032] (1) According to the ratio of 0.5 parts: 1.5 parts: 0.2 parts, 100 grams of Wuyishan Dahongpao, Anxi Tieguanyin and Chaozhou Fenghuang Dancong were quantitatively weighed, mixed, ground into tea powder, and placed in an accelerated solvent extraction device Inside;
[0033] (2) Set the extraction temperature at 20°C and the pressure at 10MPa, add 400mL of ethanol / acetone / water mixed solvent, the ratio of ethanol:acetone:water is 5:0.5:0.1, the volume ratio; static extraction 2 times, each time is 3min;
[0034] (3) Collect the extract, vacuum rotary evaporate to about 100mL, then add 30mL of acetone, place it for 10min in a low temperature environment, centrifuge at high speed, discard the precipitate, vacuum rotary evaporate the upper layer to a paste, a small amount can be used several times during the concentration Add edible alcohol to remove acetone;
[0035] (4) Dissolve the obtained ointment with 80mL of propylene glycol / alcohol / distilled water (0.5:1:5, volume...
Embodiment 2
[0037] (1) Quantitatively weigh 100 grams of Wuyishan Dahongpao, Anxi Tieguanyin, and Chaozhou Fenghuang Dancong according to the ratio of 0.7 parts: 2 parts: 0.4 parts, mix them, grind them into tea powder, and place them in an accelerated solvent extraction device Inside;
[0038] (2) Set the extraction temperature at 30°C and the pressure at 15MPa, add 600mL of ethanol / acetone / water mixed solvent, the ratio of ethanol:acetone:water is 7:1:0.5, the volume ratio; static extraction 3 times, each time is 5min;
[0039] (3) Collect the extract, vacuum rotary evaporate to about 150mL, then add 50mL of acetone, place it for 20min in a low temperature environment, centrifuge at high speed, discard the precipitate, vacuum rotary evaporate the upper layer to a paste, a small amount can be used several times during the concentration Add edible alcohol to remove acetone;
[0040] (4) Dissolve the obtained ointment with 100mL propylene glycol / alcohol / distilled water (0.7:2:7, volume r...
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