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Reactive dye

A technology for reactive dyes and dye compositions, applied in the field of reactive dyes, can solve the problems of dyes that cannot dye dark colors, high unit cost, unfavorable environmental protection, etc., and achieves good dyeing rate and fixation rate, good dyeing performance, and excellent fastness. Effect

Active Publication Date: 2009-05-27
TIANJIN DEK CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the unit cost of yellow products used in the printing and dyeing industry is high, the waste of materials is serious, salting out produces sewage, and dyes cannot dye dark colors
Moreover, the active group dyeing needs to be carried out in a strong alkaline medium, which makes it difficult to discharge the dyeing wastewater in a neutral manner, which is not conducive to environmental protection

Method used

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Examples

Experimental program
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Embodiment 1

[0016] This embodiment provides a preparation method of a specific compound in the compound of formula (I), which is a compound of the following formula (I-A):

[0017] The specific preparation method is as follows:

[0018]

[0019] 1. Diazotization of 2-naphthylamine-3,6,8-trisulfonic acid

[0020] 300kg of 70% 2-naphthylamine-3,6,8-trisulfonic acid was dropped into 500kg of water and stirred evenly, then 800kg of crushed ice was added, the temperature was 0°C, and then 200kg of 20% sodium nitrite solution was added quickly, The temperature at the end of the addition is 2°C and the stirring is continued for 2 hours, the end point temperature is 6°C with a slight excess of sodium nitrite, and the excess nitrous acid is removed with industrial sulfamic acid to prepare for coupling.

[0021] 2. Coupling:

[0022] Add 135 kg of 60% m-urea amidoaniline to 300 kg of water, stir at room temperature for 10 minutes, adjust the pH to 7.5 with 20% sodium carbonate solution, and th...

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Abstract

The invention provides a yellow active dye. A quaternary ammonium salt dye is formed by dye matrix and nicotinic acid which is an active group of the dye, can dye in neutral or alkalescent medium, and is good in each fastness index after dyeing.

Description

technical field [0001] The invention relates to the technical field of reactive dyes, in particular to a yellow reactive dye and a preparation method thereof. Background technique [0002] Reactive dyes have the characteristics of bright color, excellent application performance, and strong practicability. The active groups in the dye molecules form stable chemical bonds with the fibers and have good fastness. [0003] At present, the unit cost of yellow products used in the printing and dyeing industry is high, the material waste is serious, the salting out produces sewage, and the dye cannot dye dark colors. Moreover, active group dyeing needs to be carried out in a stronger alkaline medium, which makes it difficult to discharge dyeing wastewater neutrally and is not conducive to environmental protection. [0004] The dye provided by the invention can solve the above problems, and provides a dye that can be dyed in a weaker medium, and has good dyeing performance and can i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B62/085C09B67/22D06P3/66
Inventor 张兴华张玉卿曹世川
Owner TIANJIN DEK CHEM
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