Reactive dye
A technology for reactive dyes and dye compositions, applied in the field of reactive dyes, can solve the problems of dyes that cannot dye dark colors, high unit cost, unfavorable environmental protection, etc., and achieves good dyeing rate and fixation rate, good dyeing performance, and excellent fastness. Effect
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[0016] This embodiment provides a preparation method of a specific compound in the compound of formula (I), which is a compound of the following formula (I-A):
[0017] The specific preparation method is as follows:
[0018]
[0019] 1. Diazotization of 2-naphthylamine-3,6,8-trisulfonic acid
[0020] 300kg of 70% 2-naphthylamine-3,6,8-trisulfonic acid was dropped into 500kg of water and stirred evenly, then 800kg of crushed ice was added, the temperature was 0°C, and then 200kg of 20% sodium nitrite solution was added quickly, The temperature at the end of the addition is 2°C and the stirring is continued for 2 hours, the end point temperature is 6°C with a slight excess of sodium nitrite, and the excess nitrous acid is removed with industrial sulfamic acid to prepare for coupling.
[0021] 2. Coupling:
[0022] Add 135 kg of 60% m-urea amidoaniline to 300 kg of water, stir at room temperature for 10 minutes, adjust the pH to 7.5 with 20% sodium carbonate solution, and th...
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