Acrylic esters oiliness pressure-sensitive glue with 60 solid content and preparation method thereof
An acrylate and butyl acrylate technology, which is applied in the field of pressure-sensitive adhesives, can solve problems such as unfavorable uniform coating, surfactant precipitation, and poor water resistance, so as to reduce the amount of wet adhesive coating, increase the solid content, and reduce costs Effect
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[0020] The formula adopted in this embodiment is:
[0021] Isooctyl Acrylate 25%
[0022] Butyl Acrylate 17%
[0023] Vinyl acetate 15%
[0024] Acrylic 4%
[0025] Molecular weight regulator 5‰
[0026] Azobisisobutyronitrile 5‰
[0027] Ethyl acetate 19%
[0028] Ethanol 18%
[0029] Curing agent 5‰
[0030] Viscosity modifier 5‰
[0031] The materials selected above are all industrial grade reagents.
[0032] The preparation process steps and conditions of the present embodiment are:
[0033] Mix isooctyl acrylate, butyl acrylate, vinyl acetate, acrylic acid, molecular weight regulator, azobisisobutyronitrile, ethyl acetate and ethanol evenly according to the above raw material formula, and then add it to the reactor, and the addition amount is 100% of the reactor. 1 / 5, start heating, react at 70-85°C for 1-2 hours, add the remaining reactants dropwise and complete the dropwise addition within 2-5 hours, keep warm for 2-5 hours after the dropwise addition, and the...
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