Mineral ether-extracted Pu'er raw tea extract and preparation and use thereof
A technology of petroleum ether extraction and raw Pu'er tea, which is applied in the directions of application, preparation of tobacco, and fat production to achieve the effects of reducing irritation, enriching tobacco aroma, reducing irritation and miscellaneous gas
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Embodiment 1
[0029] Weigh 500 grams of Pu’er raw tea with an electronic balance, put it into a flask, add 2500ml of medical grade petroleum ether with a boiling point of 30-60°C, soak at 20°C for 10 hours, separate the solid and liquid with a Bush funnel, and collect the clear liquid. The obtained liquid was distilled and concentrated for 2.0 h at a vacuum degree of 0.05 MPa and a distillation temperature of 28° C., and the solvent was removed to obtain 2.4 g of extract.
Embodiment 2
[0031] Weigh 1,000 grams of Pu’er raw tea with an electronic balance, put it into an Erlenmeyer flask, add 10,000ml of petroleum ether with a boiling point of 60-90°C, soak at 30°C for 20 hours, separate the solid and liquid with a Bush funnel, and collect the clear liquid to obtain The liquid was distilled and concentrated for 1.0 h at a vacuum of 0.1 MPa and a distillation temperature of 30° C., and the solvent was removed to obtain 13.50 g of extract.
Embodiment 3
[0033] Weigh 1,000 grams of Pu’er raw tea with an electronic balance, put it into an Erlenmeyer flask, add 15,000ml of petroleum ether with a boiling point of 30-60°C, soak at 15°C for 10 hours, separate the solid and liquid with a Bush funnel, and collect the clear liquid to obtain The liquid was distilled and concentrated for 1.5 h at a vacuum of 0.01 MPa and a distillation temperature of 25° C., and the solvent was removed to obtain 13.60 g of extract.
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