Process for recovering ethanol in gruffs
A technology for recovering ethanol and ethanol, which is applied in chemical instruments and methods, preparation of organic compounds, organic chemistry, etc., can solve the problems of increased loss, difficulty in direct use, and high cost of ethanol use, so as to reduce waste and shorten Production cycle, to achieve the effect of repeated use
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Embodiment 1
[0013] After 1000 kilograms of ginkgo leaves are extracted with 80% ethanol and the medicinal solution is exhausted, the residue contains about 1200L of ethanol (95% concentration)
[0014] (1) Dry recovery: open the steam valve leading into the extraction tank, directly pass steam to the bottom of the medicinal residue for steam distillation to recover ethanol, the distilled ethanol enters the high-concentration ethanol storage tank through the cooling system; the ethanol concentration to be distilled When it is 70-75%, stop heating, recover about 1000L of 80% ethanol, convert 95% to about 840L, which can be directly used as the next batch of extraction solvent.
[0015] If the medicinal materials are fine leaves or powder, the recovery ability of the dry method is average, and the recovery rate can reach more than 70%; if the medicinal materials are granules or decoction pieces, the recovery ability of the dry method is stronger, and the recovery rate can reach more than 80%....
Embodiment 2
[0024] After 2000 kg of Corydalis Corydalis is extracted with 70% ethanol and the liquid is exhausted, the residue contains about 1000L of ethanol (95% concentration):
[0025] (1) Dry recovery: open the steam valve leading into the extraction tank, directly pass steam to the bottom of the medicinal residue for steam distillation to recover ethanol, the distilled ethanol enters the high-concentration ethanol storage tank through the cooling system; the ethanol concentration to be distilled After 60-65%, stop heating;
[0026] The ethanol recovered in this process is 1150L in total, with a concentration of 69%, or 835L after 95% conversion, which is basically the same depth as the ethanol used for extraction, and can be directly used as the next batch of extraction solvent. Strong, the recovery rate can reach more than 80%.
[0027] (2) Wet recovery: Add drinking water from the bottom of the extraction tank to submerge the surface of the dregs, open the steam valve leading to ...
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