Modification method for nano-titanium dioxide on natural stone surface
A nano-titanium dioxide and stone technology, applied in the application field of nano-coating materials, can solve problems such as low quantum efficiency, achieve low water absorption, excellent stain resistance, and a wide range of applications
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[0030] The present invention adopts the method of low-temperature chemical modification, and first adopts the sol-gel method to prepare TiO with a molar concentration of 2mol / L and a particle size of about 10nm. 2 Transparent sol, the specific preparation method is: respectively take TiCl with a concentration of 2.2mol / L 4 Put 40mL and 80mL of the solution in two 1000mL beakers, dilute with 350mL of distilled water, then use 1:20 ammonia water to adjust the pH value to between 9 and 10, a large amount of precipitates are generated, filter and wash with suction until the washing solution is tested with silver nitrate solution No Cl - exist, then add 60mL, 120mL 30% H 2 o 2 When a clear brown-yellow sol appeared, add 0.1mL and 0.2mL H 3 PO 4 , sieved with a 300-mesh sieve, then moved to a 1000ml three-necked flask, refluxed at a constant temperature of 80°C for 3h, refluxed at 90°C for 5h, and cooled naturally to obtain anatase nano-TiO 2 Sol.
[0031] Then the prepared Ti...
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