Production process of super strength interference pearlylustre pigment
A production process, pearlescent pigment technology, applied in the direction of inorganic pigment treatment, fibrous filler, dyeing physical treatment, etc., can solve the problems of complex production process, high cost, difficult process, etc., achieve simple production process, low production cost, easy operation convenient effect
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Embodiment 1
[0022] Add 15g of synthetic 10-40μm mica, add soft water to make the solid-liquid ratio 1:6, and the reaction temperature is 85°C, stir evenly, and then coat;
[0023] The first layer, with a concentration of 20wt% NaOH solution to adjust the pH value to 2.3, 25.88g of TiCl 4 After dissolving in 250ml of demineralized water, add it slowly in parallel flow with 20% NaOH solution, and keep the pH value at 2.3;
[0024] In the second layer, 8.75g FeCl 3 ·6H 2 O and 1.7 g TiCl 4 Dissolve in 120ml and 18ml of soft water respectively, then mix evenly, and slowly add in the same amount of NaOH solution with a concentration of 20wt%, adjust the pH value to 4, stir for 30 minutes, let stand for 1 hour, and adjust the solid-liquid ratio to 1:13 , with a mass ratio of 30wt% hydrochloric acid to adjust the pH value to 1.2;
[0025] In the third layer, 1.80g SnCl 2 After dissolving in 20ml of soft water, add it slowly in parallel with 20wt% NaOH solution, and keep the pH value at 1.5;...
Embodiment 2
[0029] Add 19g of synthetic 10-40μm mica, add soft water to make the solid-liquid ratio 1:16, and the reaction temperature is 85°C, stir evenly, and then coat;
[0030] The first layer, with a concentration of 20% NaOH solution to adjust the pH value to 2.3, 36.8g of TiCl 4 After dissolving in 350ml soft water, with the concentration of 25wt% NH 3 ·H 2 O solution is added slowly in parallel flow to keep the pH value at 2.3; stop adding TiCl when the quality of the coating film reaches 172.5% of the amount of mica input 4 soft aqueous solution;
[0031] In the second layer, 11.4g FeCl 3 ·6H 2 O and 2.50 g TiCl 4 Dissolve in 150ml and 22ml soft water respectively, then mix evenly, and mix with 25wt% NH 3 ·H 2 The O solution is added slowly in parallel flow, the pH value is adjusted to 4, stirred for 30 minutes, allowed to stand for 1 hour, the solid-liquid ratio is adjusted to 1:13, and the pH value is adjusted to 1.2 with 30% hydrochloric acid by mass ratio;
[0032] In...
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