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Carbon nano-tube thin film structure and preparation method thereof

一种碳纳米管薄膜、薄膜结构的技术,应用在纳米结构制造、定向碳纳米管、纳米技术等方向,能够解决不利碳纳米管性能、碳纳米管聚集成团、薄膜厚度不均等问题,达到良好机械强度及韧性、方便应用、体积比小的效果

Active Publication Date: 2008-08-13
TSINGHUA UNIV +1
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Problems solved by technology

[0005] However, in the above-mentioned carbon nanotube film structure obtained by direct growth method or spraying method, carbon nanotubes are often easily aggregated into agglomerates, resulting in uneven film thickness.
The structure of the above-mentioned carbon nanotube film prepared by the LB method is generally a uniform network structure, and the carbon nanotubes are uniformly dispersed and not agglomerated. However, the carbon nanotubes are still arranged in disorder in the film, which is not conducive to fully utilizing the carbon nanotubes. performance, its application is still limited

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  • Carbon nano-tube thin film structure and preparation method thereof
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  • Carbon nano-tube thin film structure and preparation method thereof

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preparation example Construction

[0015] see figure 1 , the preparation method of the carbon nanotube thin film structure of the embodiment of the present invention mainly includes the following steps:

[0016] Step 1: providing a carbon nanotube array, preferably, the array is a super-aligned carbon nanotube array.

[0017] In this embodiment, the preparation method of the super-parallel carbon nanotube array adopts the chemical vapor deposition method, and its specific steps include: (a) providing a flat substrate, which can be a P-type or N-type silicon substrate, or a silicon substrate formed with The silicon base of oxide layer, present embodiment preferably adopts the silicon base of 4 inches; (b) uniformly form a catalyst layer on the base surface, this catalyst layer material can be selected iron (Fe), cobalt (Co), nickel (Ni) or one of alloys in any combination thereof; (c) annealing the above-mentioned substrate formed with a catalyst layer in air at 700-900° C. for about 30 minutes to 90 minutes; (...

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Abstract

The present invention provides a preparing method of carbon nanotube film structure, including following steps: providing a carbon nanotube array; adopting a pulling tool to acquire at least two carbon nanotube films from the carbon nanotube array; providing a fixed frame, forming a multiple-layer carbon nanotube film structure by overlap adhereing the carbon nanotube film in the fixed frame; and treating the multiple-layer carbon nanotube film by an organic solvent. The carbon nanotube film structure prepared by the method includes at least two layers overlapped and cross-over installed carbon nanotube film, which includes multiple carbon nanotube bundle end to end and arranged in the direction, the multiple-layer carbon nanotube film further includes millipore crosswise formed by multiple carbon nanotube bundles.

Description

technical field [0001] The invention relates to a carbon nanotube film structure and a preparation method thereof. Background technique [0002] Carbon nanotubes are a new type of one-dimensional nanomaterials discovered in the early 1990s. The special structure of carbon nanotubes determines its special properties, such as high tensile strength and high thermal stability; with the change of the helical mode of carbon nanotubes, carbon nanotubes can exhibit metallic or semiconducting properties. Because carbon nanotubes have an ideal one-dimensional structure and excellent properties in the fields of mechanics, electricity, and heat, they have shown broad application prospects in interdisciplinary fields such as materials science, chemistry, and physics. They are widely used in scientific research and industrial applications. has also received increasing attention. [0003] Although carbon nanotubes have excellent properties and are widely used, generally the prepared carb...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/02B82B3/00B82B1/00
CPCY10T428/249964Y10T428/24074Y10T428/24058B82Y40/00B32B2313/04Y10T428/249982B32B2457/00B32B2305/38C01B31/0253Y10T428/249978Y10T428/249953Y10T156/1092B32B38/10C01B2202/08B82Y30/00Y10T428/30Y10T156/1089B32B2309/02Y10T428/249962Y10S977/742Y10T428/24124B32B2309/105C01B32/168
Inventor 冯辰姜开利刘亮张晓波范守善
Owner TSINGHUA UNIV
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