Novel use of fraxinellone and fraxinellone aqua pesticide
An insecticide and a technology for preparing insecticides, applied in the direction of nematicides, applications, biocides, etc., can solve problems such as unseen research, and achieve an effect that is conducive to environmental protection and ecological balance
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[0017] 1, the extraction method of arketone in the white moss bark.
[0018] Weigh 10 kg of white moss bark powder, moisten with 10 times the amount of lye without sticking hands, add an appropriate amount of petroleum ether to soak for 24 hours, add 10 times the amount of petroleum ether to reflux extraction three times, each time for 1.5 hours, and suction filter. The filtrates were combined and concentrated to dryness to obtain a petroleum ether extract. Add the above extract to a mixed solvent of methanol:petroleum ether=3:1, separate with a separatory funnel, discard the fat-soluble components in the upper layer, and the white needle-like crystals will crystallize from the methanol in the lower layer solution, and recrystallize through methanol to obtain ash Crude ketones.
[0019] The crude product was further purified by column chromatography using cyclohexane: ethyl acetate = 3:2 as the eluent and recrystallized from methanol to obtain the fine alkone. The content of...
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