Carboxymethyl chitosan fruit preserving coating agent and preparation method thereof
A technology of carboxymethyl chitosan and film coating agent, which is applied in the fields of fruit and vegetable preservation, protection of fruits/vegetables with a coating protective layer, food preservation, etc., and can solve the complex production process of preservatives, easy to produce peculiar smell, and fruit chilling damage and other problems, to achieve the effect of reducing the respiration of fruits, increasing the brightness of fruits, and enhancing the blocking effect
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Embodiment 1
[0025] Make 2 kilograms of carboxymethyl chitosan fruit fresh-keeping coating agent, its proportioning is as follows: N, O-carboxymethyl chitosan 2%, glycerin 0.5%, Tween 80 is 1.2%, DL-α-acetic acid fertile 0.5% phenol, 95.8% water.
[0026] Weigh 40 grams of carboxymethyl chitosan, 10 grams of glycerin, 24 grams of Tween 80, 10 grams of DL-α-tocopheryl acetate, and 1916 grams of water. Put 1916 grams of water in a 45-55°C water bath and heat to a constant temperature, add 40 grams of carboxymethyl chitosan, and stir until completely dissolved. Then add 10 grams of glycerin, 24 grams of Tween 80 and stir evenly, then add 10 grams of DL-α-tocopheryl acetate and stir until completely dissolved. Then, put it at room temperature to cool naturally, and then filter to remove undissolved substances, and degas under 0.1-0.5MPa vacuum for 2h. Stand overnight at room temperature, degas again under 0.1 MPa vacuum for 2 hours, and let stand at room temperature for 1 hour to obtain 2 kg...
Embodiment 2
[0030] Make 2 kilograms of carboxymethyl chitosan fruit fresh-keeping coating agent, its proportioning is as follows: N, O-carboxymethyl chitosan 4%, glycerol 1%, Tween 80 is 2%, DL-α-acetic acid fertile 1% phenol, 92% water.
[0031] Weigh 80 grams of carboxymethyl chitosan, 20 grams of glycerin, 40 grams of Tween 80, 20 grams of DL-α-tocopheryl acetate, and 1840 grams of water. Put 1840 grams of water in a 45-55°C water bath and heat to a constant temperature, add 80 grams of carboxymethyl chitosan, and stir until completely dissolved. Then add 20 grams of glycerin, 40 grams of Tween 80 and stir evenly, then add 20 grams of DL-α-tocopheryl acetate and stir until completely dissolved. Then, put it at room temperature to cool naturally, and then filter to remove undissolved substances, and degas under 0.1-0.5MPa vacuum for 2h. Stand overnight at room temperature, degas again under 0.1 MPa vacuum for 2 hours, and let stand at room temperature for 1 hour to obtain 2 kg of carb...
Embodiment 3
[0035] Make 2 kilograms of carboxymethyl chitosan fruit fresh-keeping coating agent, its proportioning is as follows: N, O-carboxymethyl chitosan 0.5%, glycerin 0.1%, Tween 80 is 0.3%, DL-α-acetic acid fertile Phenol 0.1%, water 99%.
[0036] Weigh 10 grams of carboxymethyl chitosan, 2 grams of glycerin, 6 grams of Tween 80, 2 grams of DL-α-tocopheryl acetate, and 1980 grams of water. Put 1980 grams of water in a 45-55°C water bath and heat to a constant temperature, add 10 grams of carboxymethyl chitosan, and stir until completely dissolved. Then add 2 grams of glycerin, 6 grams of Tween 80 and stir evenly, then add 2 grams of DL-α-tocopheryl acetate and stir until completely dissolved. Then, put it at room temperature to cool naturally, and then filter to remove undissolved substances, and degas under 0.1-0.5MPa vacuum for 2h. Stand overnight at room temperature, degas again under 0.1 MPa vacuum for 2 hours, and let stand at room temperature for 1 hour to obtain 2 kg of ca...
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