Method for preparing activated charcoal by using discarded edible mushroom slag
A technology for preparing activated carbon and fungus residue, which is applied in the field of utilization of waste edible fungus residue, can solve the problems of unreasonable utilization and limited ability to deal with fungus residue, and achieve the effects of eliminating environmental pollution, obvious market competitive advantages, and rich sources of raw materials
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Embodiment 1
[0032] Sieve the waste edible mushroom residue with a 3-20 mesh sieve to remove sand, soil and other impurities, and then pickle it with 20% nitric acid solution at a temperature of 45°C for 10 hours; The bacterium slag after the washing process is dried in a dryer, so that the moisture content of the dried bacterium slag is 20%, and then it is pulverized into powder with a particle size of 80 meshes; In terms of weight percentage, add 15% coal tar, stir and mix evenly, put it into a molding machine to make pellets with a particle size of 8mm, and then under the protection of an inert gas, heat up to 550°C at a rate of 20°C / min for carbonization , The carbonization time is 1 hour; the carbonized material is activated with carbon dioxide gas at a temperature of 800 ° C for 60 minutes. The yield of activated carbon is 30%, the iodine adsorption value is 800mg / g, and the strength of activated carbon is 90%.
Embodiment 2
[0034] Sieve the waste edible mushroom residue with a 3-20 mesh sieve to remove sand, soil and other impurities, and then pickle it with a nitric acid solution with a concentration of 30% at a temperature of 60°C for 3 hours; The bacterium slag after the washing process is dried in a dryer, so that the moisture content of the dried bacterium slag is 8%, and then it is pulverized into powder with a particle size of 50 mesh; In terms of weight percentage, add 20% polyvinyl alcohol, stir and mix evenly, put it into a molding machine to form a column with a diameter of 8mm, and then under the protection of an inert gas, raise the temperature to 600°C at a rate of 15°C / min for carbonization. The carbonization time is 1.5 hours; the carbonized material can be activated with carbon dioxide gas for 120 minutes at a temperature of 750°C. The yield of activated carbon is 27%, the iodine adsorption value is 900mg / g, and the strength of activated carbon is 85%.
Embodiment 3
[0036] Sieve the waste edible mushroom residue with a 3-20 mesh sieve to remove sand, soil and other impurities; dry the screened mushroom residue in a dryer so that the moisture content of the dried mushroom residue is 12%. Then it is pulverized into a powder of 100 mesh particle diameter; the particle diameter is 100 mesh powdery bacterium residue, by weight percentage, add 10% phenolic formaldehyde and stir and mix evenly, put into the forming machine and make a columnar shape with a diameter of 4mm, Then, under the protection of inert gas, carbonize at a rate of 10°C / min to 400°C for 2.5 hours; activate the carbonized material with water vapor at a temperature of 800°C for 80 minutes. The yield of activated carbon is 32%, the iodine adsorption value is 720mg / g, and the strength of activated carbon is 90%.
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