Method for detecting oxidation preventive content in jet fuel
An anti-oxidant and jet fuel technology, applied in the direction of material electrochemical variables, test sample preparation, etc., to achieve the effect of portability, easy operation, and less impact
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Embodiment 1
[0032] The No. 3 jet fuel containing the antioxidant 2,6-di-tert-butyl-p-cresol and the concentration in the range of 10mg / L-30mg / L was used as the sample to be tested.
[0033] Measuring conditions: instrument: electrochemical analyzer; electrode system: 3mm glassy carbon working electrode, Ag / AgCl non-aqueous reference electrode, 0.5mm platinum wire auxiliary electrode; electrolyte system: 0.1M KOH ethanol solution; initial voltage -0.1V, Termination voltage +0.5V, voltage increment 0.002V, amplitude 0.05V, pulse width 0.06s, sampling width 0.02s, rest time 2.0s, sensitivity 1×10 -5 .
[0034] Determination steps:
[0035] Firstly, the standard sample of antioxidant 2,6-di-tert-butyl-p-cresol was electrochemically analyzed.
[0036] Preparation of reserve standard sample: Accurately weigh 0.05g 2,6-di-tert-butyl-p-cresol in a 50ml beaker, add a little jet fuel identical to the sample, dissolve, and transfer to a 100ml volumetric flask, constant volume, to obtain The 2,6-d...
Embodiment 2
[0045] Embodiment 2: sample analysis to be tested
[0046] In the analysis of the sample to be tested, the steps are the same as in Example 1, the only difference being that the standard sample is changed to the sample to be tested.
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