Compositions useful to provide improved rheology and mist control to ink formulations and ink formulations containing such compositions
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example 1
Preparation of the Polyamide Reaction Product
[0043] Empol® 1061 (792.9 grams) was placed in a 2 liter, 4-neck, preweighed reactor equipped with a Barrett distilling receiver and a Friedrichs condenser. The Empol® 1061 was heated to 100° C. and then diethylenetriamine (190.6 grams) was added. The contents were heated to 240° C. under a nitrogen blanket while mixing at 300 RPM. A reaction occurred with the liberation of water, which was collected in a receiver. The reaction was allowed to continue until the acid value was ≦2.0 (mg KOH / gram of reaction mixture). The reaction was halted and the reactor reweighed.
example 2
[0044] Product of Example 1 was allowed to cool to 80° C. under agitation. Reaction product in Example 1 (65 parts) was mixed with tridecyl alcohol (35 parts). The composition was mixed for 15 minutes. The resulting product was poured into an appropriate storage container.
example 2a
[0045] The reaction product of example 1 (65 parts) was mixed slowly at 500 RPM with polypropylene glycol MW 425 (35 parts). The composition was mixed for 15 minutes. The resulting product was poured into an appropriate storage container.
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