Lozenge and its preparing method
An extraction method and technology of raw materials, which are applied in the field of lozenges with the effect of relieving throat and promoting body fluid and their preparation, can solve the problems of single, incomplete extraction of active ingredients, and numerous processes
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Embodiment 1
[0034] Take the following weights of ingredients:
[0035] 70g honeysuckle, 60g fat sea, 36g dark plum, 15g citric acid, 1.8g menthol, 240g sorbitol, 200g soluble starch, 120g D-mannitol, 1.8g sweetener, 7.45g magnesium stearate,
[0036] Prepare as follows:
[0037] A. Extraction:
[0038] Take honeysuckle, boil and extract twice, respectively for 1 hour, filter, combine the two filtrates, concentrate to a relative density of 1.10 at 80°C, add ethanol until the alcohol content is 60%, settle for 8 hours, take the supernatant, sediment Wash with 60% ethanol, combine the supernatant and the ethanol washing liquid and recover the ethanol, continue to concentrate to a relative density of 1.20 at 80°C, dry, pulverize, and pass through an 80-mesh sieve;
[0039] Take Panda Dahai, soak in hot water at 90°C for 4 times, 1 hour each time, filter, combine the filtrates from 4 times, concentrate to a relative density of 1.18 at 80°C, dry, crush, and pass through an 80-mesh sieve;
[...
Embodiment 2
[0045] Take the following weights of ingredients:
[0046] 20g honeysuckle, 20g fat sea, 100g dark plum, 8g citric acid, 1g menthol, 160g sorbitol, 100g D-mannitol, 150g soluble starch, 1g sweetener, 8g magnesium stearate,
[0047] Prepare as follows:
[0048] A. Extraction:
[0049] Take honeysuckle, boil and extract 3 times, respectively for 1 hour, filter, combine the filtrates, concentrate to a relative density of 1.11 at 80°C, add ethanol to 50% alcohol content, settle for 48 hours, take the supernatant, and use 50 Wash with % ethanol, combine the supernatant and the ethanol washing solution and recover ethanol, continue to concentrate to a relative density of 1.10 at 80°C, and spray dry;
[0050] Take Panda Dahai, soak in hot water at 80°C for 6 times, half an hour each time, filter, combine the filtrates, concentrate to a relative density of 1.11 at 80°C, and spray dry;
[0051] Take ebony, boil and extract 3 times, each time for 1 hour, filter, combine the filtrates...
Embodiment 3
[0056] Take the following weights of ingredients:
[0057] 200g honeysuckle, 200g fat sea, 10g black plum, 22g citric acid, 3g menthol, 200g sorbitol, 250g soluble starch, 130g D-mannitol, 2g sweetener, 12g magnesium stearate,
[0058]Prepare as follows:
[0059] A. Extraction:
[0060] Take honeysuckle, boil and extract once, separate for 2 hours, filter, concentrate the filtrate to a relative density of 1.12 at 80°C, add ethanol until the alcohol content is 80%, settle for 20 hours, take the supernatant, and use 80% ethanol for the sediment Wash, combine the supernatant and ethanol washing solution and recover ethanol, continue to concentrate to a relative density of 1.22 at 80°C, dry, pulverize, and pass through an 80-mesh sieve;
[0061] Take Panda Dahai, soak it twice in hot water at 90°C for 1 hour each time, filter, combine the filtrates, concentrate to a relative density of 1.21 at 80°C, dry, crush, and pass through an 80-mesh sieve;
[0062] Take ebony, boil and ex...
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