Predextrinization acetylated distarch phosphate and its preparation method
A technology for pregelatinizing acetylated distarch phosphate and acetylated distarch phosphate, which is applied in the field of pregelatinizing acetylated distarch phosphate and its preparation, can solve problems such as poor water retention capacity and poor transparency, and achieve good water absorption. , The product has good application effect and strong water retention ability.
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Embodiment 1
[0029] First, 100 kg of waxy starch, 10 kg of sodium sulfate, and 180 kg of water were adjusted into a 20-23Be starch slurry in the reactor, stirring continuously, and 3-3.8% sodium hydroxide solution was added to the kettle to adjust the pH value to 11.5, and 0.06 Kg of sodium trimetaphosphate, heat up to 45°C, react for 4 hours, cool down to 20°C, adjust the pH value to 8.5-9.0 with 8-10% hydrochloric acid, add 4.5 kg of acetic anhydride, keep the temperature at 20±1°C to react, During the reaction process, continuously add 3-3.8% sodium hydroxide solution dropwise to maintain a pH value of 8.5. After the addition of acetic anhydride, continue to react for 1 hour, add 8-10% hydrochloric acid solution to neutralize to a pH value of 6.0-7.0, and pour into the kettle Add 200 kg of water to wash and settle, and then wash and settle in the same way to remove impurities (sodium sulfate, sodium chloride or other chemical residues) to obtain the initial product of acetate starch, and...
Embodiment 2
[0031] The steps are the same as in Example 1, except that the pH value of the esterification process is maintained at 8.0, and the reaction temperature is maintained at 20±1°C.
Embodiment 3
[0033] The steps are the same as in Example 1, except that the pH value of the esterification process is maintained at 8.5, and the reaction temperature is maintained at 25±1°C.
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