Method of preparing adsorbent of heavy metal ion
A technology of heavy metal ions and adsorbents, applied in the direction of non-metallic elements, chemical instruments and methods, molecular sieve compounds, etc., can solve the problems of limiting adsorbents, and achieve the effects of simple operation, high mechanical stability, and high hydrothermal stability
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Embodiment 1
[0021] Under stirring at 55°C, 1.0 g of nonionic polymer C 18 h 37 (OCH 2 CH 2 ) 10 OH (Brij-76) was dissolved in 8.0 g deionized water and 16.0 g 2M HCl, after the solution was clear, 1.215 g (MeO) was added 3 SiCH 2 CH 2 Si(OMe) 3 and 0.098g(MeO) 3 SiCH 2 CH 2 CH 2 SH, aging with stirring for more than 24h, crystallized at 55°C for 16h. After the product was filtered, washed with water and dried, it was extracted with a mixed solution of 160ml of absolute ethanol and 1g of HCl at 55°C for 6h to obtain an organic / inorganic hybrid mesoporous material containing -SH adsorption center. The samples were tested by XRD, N 2 Adsorption / desorption, TEM characterization confirmed a highly ordered two-dimensional hexagonal phase structure. The BET specific surface area of the material is 1011m 2 / g; the pore volume is 0.86cm 3 / g; the channel size is 3.40nm. Wherein the S content is 0.68mmol / g.
Embodiment 2
[0023] Adopt the preparation process of embodiment 1, add 1.08g (MeO) 3 SiCH 2 CH 2 Si(OMe) 3 and 0.196g(MeO) 3 SiCH 2 CH 2 CH 2 SH as silicon source. Stir at room temperature for 72 hours, and crystallize at 100°C for 24 hours. The specific surface area of the obtained material is 958m 2 / g; the pore volume is 0.67cm 3 / g; the channel size is 2.20nm. Wherein the S content is 1.69mmol / g.
Embodiment 3
[0025] Adopt the preparation process of embodiment 1, add 0.945g (MeO) 3 SiCH 2 CH 2 Si(OMe) 3 and 0.294g(MeO) 3 SiCH 2 CH 2 CH 2 SH as silicon source. The product was extracted with a mixed solution of 120ml of absolute ethanol and 2.4g of HCl at 60°C for 3 hours, and the specific surface area of the obtained material was 673m 2 / g; the pore volume is 0.41cm 3 / g; the channel size is 1.69nm. Wherein the S content is 2.12 mmol / g.
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