Flax viscose filaments and their preparation
A technology of viscose filament and hemp material, which is applied in the direction of artificial filament made of viscose, and can solve problems such as uncomfortable wearing, failure to achieve the purpose of antibacterial, and allergic reactions
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Embodiment 1
[0014] (1) The quality of the pulp used: methyl fiber 95.2%, viscosity 10.0mpa.s, ash content 0.12%, iron content 21ppm, whiteness 79%, alkali absorption value 600%
[0015] (2) Impregnation: lye concentration 220g / l, lye temperature 22°C, immersion time 140 minutes
[0016] (3) Aging: Aging temperature 27℃, electron beam energy 20KG, methyl fiber 31%, caustic soda content 16%
[0017] (4) Yellowing: adding amount of dissolved alkali (p-methyl cellulose) 75%, dissolving alkali time 25 minutes, adding amount of carbon disulfide (p-methyl cellulose) 42%, yellowing time 70 minutes, adding amount of sulfanilamide 1.5%, initial yellowing temperature 20°C The final yellowing temperature is 32°C.
[0018] (5) Post-dissolution: methyl cellulose 7.8%, caustic soda 5.5%, maturity 8ml, viscosity 40s
[0019] (6) Spinning: acid bath composition sulfuric acid: 120g / l zinc sulfate 9g / l sodium sulfate 290g / l butane 4-carboxylic acid 0.5‰ temperature 48°C
[0020] (7) Finished product qual...
Embodiment 2
[0032] (1) The quality of the pulp used is: methyl cellulose 96.0%, viscosity 11.7mpa.s, ash content 0.10%, iron content 24ppm, whiteness 80%, alkali absorption value 700%
[0033] (2) Impregnation: lye concentration 240g / l, lye temperature 18°C, immersion time 120 minutes
[0034] (3) Aging: Aging temperature 22°C, electron beam energy 10KG, methyl fiber 32.5%, caustic soda content 17.3%
[0035] (4) Yellowing: adding amount of dissolved alkali (p-methyl cellulose) 70%, dissolving alkali time 30 minutes, adding amount of carbon disulfide (p-methyl cellulose) 40%, yellowing time 90 minutes, adding amount of p-aminobenzenesulfonamide 1.0% yellowing initial temperature 18°C The final yellowing temperature is 30°C.
[0036] (5) Post-dissolution: methyl cellulose 8.6%, caustic soda 5.90%, maturity 12ml, viscosity 25S
[0037] (6) Spinning: acid bath composition sulfuric acid: 140g / l zinc sulfate 13g / l sodium sulfate 250g / l butane 4-carboxylic acid 1.5‰ temperature 54°C
[0038]...
Embodiment 3
[0050] (1) The quality of the hemp pulp used is: cellulose 95.0%, viscosity 14.0mpa.s, ash content 0.09%, iron content 25ppm, whiteness 78%, alkali absorption value 500%
[0051] (2) Impregnation: lye concentration 260g / l, lye temperature 16°C, immersion time 100 minutes
[0052] (3) Aging: Aging temperature 25℃, electron beam energy 15KG, methyl fiber 34%, caustic soda content 19%
[0053] (4) Yellowing: adding amount of dissolved alkali (p-methyl cellulose) 65%, time for dissolving alkali 35 minutes, adding amount of carbon disulfide (p-methyl cellulose) 38%, yellowing time 110 minutes, adding amount of p-aminobenzenesulfonamide
[0054] 0.5% The initial yellowing temperature is 16°C and the final yellowing temperature is 28°C.
[0055] (5) Post-dissolution: cellulose 8.2%, caustic soda 5.75%, maturity 10ml, viscosity 30S
[0056] (6) Spinning: acid bath composition sulfuric acid: 130g / l zinc sulfate 11g / l sodium sulfate 270g / l butane 4-carboxylic acid 1.0‰ temperature 51°...
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