Method of supercritical CO2 for extracting effective constituent from whole spores of ganoderma lucidum
A technology of Ganoderma lucidum spores and active ingredients, which is applied to medical preparations containing active ingredients, solid solvent extraction, pharmaceutical formulations, etc., can solve problems such as affecting extraction efficiency, and achieve high extraction efficiency, energy saving, and simple process flow. Effect
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Embodiment 1
[0022] Put 10 kg of Ganoderma lucidum fruiting body and 20 kg of Ganoderma lucidum spores crushed into 200 meshes into extraction kettle 1, and introduce CO 2 , the control temperature is 32°C, the pressure is 12Mpa, and the time is 4 hours, the CO containing whole Ganoderma lucidum spore extract that flows out from said extraction kettle 1 2 into the separation tank 2, CO 2 Flow out from the separation kettle 2 tops, and 1.6 kilograms of whole Ganoderma lucidum spore extracts in oil and paste state flow out from the vacuum separator 2 bottoms.
[0023] Among them: polysaccharide is 0.36%, and triterpene is 8.07%.
Embodiment 2
[0025] Put 20 kg of Ganoderma lucidum fruiting bodies and 10 kg of Ganoderma lucidum spores into extraction kettle 1 with 400 meshes, and inject CO 2 , the control temperature is 48°C, the pressure is 30Mpa, and the time is 5 hours, the CO containing the whole Ganoderma lucidum spore extract flowing out from said extraction kettle 1 2 Into vacuum separator 2, CO 2 Flow out from the vacuum separator 2 tops, and 1.2 kilograms of whole Ganoderma lucidum spore extracts in oil and paste state flow out from the vacuum separator 2 bottoms.
[0026] Among them: polysaccharide is 2.33%, and triterpene is 12.16%.
Embodiment 3
[0028] Adopt the same method as Example 1, but when extracting, add 3 kilograms of edible ethanol with a weight concentration of 70% as a carrier agent to obtain 2.5 kilograms of whole Ganoderma lucidum spore extract in oil and paste state, wherein: polysaccharide is 1.28% , triterpenes are 11.24%.
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