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Extracting method of polyphenol from lotus root

An extraction method and technology of lotus root, applied in the field of extraction of polyphenols from lotus root, can solve the problems of high cost and high production conditions, and achieve the effect of rich nutrition and scavenging free radicals in human body

Inactive Publication Date: 2004-02-04
WUHAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the production of this process requires relatively large-scale production equipment, the cost is expensive, and the production conditions are relatively high.

Method used

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  • Extracting method of polyphenol from lotus root

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Embodiment Construction

[0022] according to figure 1 The present invention is described in further detail:

[0023] according to figure 1 It can be seen that lotus leaf crushing 1 obtains lotus leaf wood 2. Take 20 g of lotus leaf powder, add 160 ml of 70% ethanol solution, adjust the pH to 3, stir and extract in a water bath at 70 ° C (the time is 1 h, 2 h, and 3 h respectively), combine the three filtrates, filter, and discard the filter residue 3, Keep the filtrate 4; adjust the pH of the filtrate to 11, concentrate in a water bath at 70°C until the ethanol is evaporated to remove the concentrated solution 5; then adjust the pH of the concentrated solution to 3 to convert the chlorophyll into water-insoluble pheofolate and remove Precipitate 6, retain the aqueous layer 7. The aqueous layer was extracted twice with twice as much ethyl acetate, the aqueous layer 8 was discarded, and the ethyl acetate layer 9 was retained; the ethyl acetate was evaporated and vacuum-dried to obtain 2.2 g of light ...

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Abstract

A process for extracting polyphenol from lotus root includes such steps as pulverizing lotus root, immersing in alcohol solution, heating while stirring, filtering, thermal concentrating, extracting with ethyl acetate, concentrating, drying to obtain coarse product, dissolving in acetone solution, separating and purifying. Its advantages are high quality of product, low cost and no pollution.

Description

Technical field: [0001] The invention relates to the field of biotechnology, in particular to a method for extracting polyphenols from lotus root. Background technique: [0002] As early as the early 1960s, Japanese scientists discovered that tea contains a large number of substances with strong antioxidant activity - tea polyphenols. By the 1980s, the preparation technology of tea polyphenols had made great progress and entered the practical stage of industrial production. At present, there are nearly ten varieties of tea antioxidant products sold in the international market in three dosage forms (water-based, oil-based, powder-based). Since the 1990s, my country has successively developed several tea polyphenol extraction processes and their products, and carried out industrial production. [0003] Lotus root is an important economic crop in China. In the past ten years, the planting area in my country has increased rapidly. There are a lot of polyphenols in lotus root....

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D11/02C07D311/30C07D311/62
Inventor 靳素荣丁佑铭周明全胡中立余作平
Owner WUHAN UNIV
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