Protein synthetic fiber and its production method
A technology for synthetic fibers and manufacturing methods, applied in the direction of cellulose/protein conjugated rayon, etc., can solve the problems of inability to guarantee fiber quality, trouble, protein loss, etc. The effect of mutual solubility
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Embodiment 1
[0023] Embodiment 1: Add the alkaline solution that the pH value is 9.6 to the soya bean that soaks in water and grind by wet method, dissolve under the condition that temperature is 29 ℃, material-water ratio is 1: 15, and dissolution time is 180 minutes, put Add gelatin to an alkaline solution with a pH value of 9.6, and dissolve it at a temperature of 28°C. The ratio of material to water is 1:40, and the dissolution process takes 240 minutes. The dissolution process should be stirred, then allowed to stand and separated to remove waste residue. To obtain the leachate, add hydrochloric acid in the leachate, adjust the isoelectric point of the leachate to obtain the isolated protein; the prepared plant protein isolate and animal protein isolate are dissolved in triethanolamine-containing triethanolamine with a pH value of 12 at a dry solid weight ratio of 1:29 In the aqueous solution, the initial temperature of dissolution is 30°C, then heated to 91°C, then the temperature is ...
Embodiment 2
[0025] Example 2: Put the crushed and defatted soybeans and cheese protein into a solution with a pH value of 7.8, and dissolve them at a temperature of 28°C. The dissolution time is 120 minutes. The dissolution process should be stirred, and then allowed to stand , separate and remove the waste residue to obtain leachate, add phosphoric acid in the leachate to adjust the isoelectric point to obtain isolated protein, and dissolve the two isolated proteins in a solution containing triethanolamine with a pH value of 1.5 at a ratio of 5:21. The temperature is 40°C, then heated to 95°C, and kept at 95°C for 20 minutes to make a protein solution with a concentration of 5% As; add polyvinyl alcohol (PVA) that has been washed into the protein solution, Make it blend and copolymerize at a temperature of 95°C, raise the temperature to 98°C and keep it for 60 minutes to make a spinning solution containing animal and vegetable protein and polyvinyl alcohol, and adjust the solution to a co...
Embodiment 3
[0027] Embodiment 3: Put the degreased cottonseed meal into a solution with a pH value of 9.5, and dissolve it at a temperature of 29.5°C. The ratio of material to water is 1: 15, and the dissolution time is 70 minutes. The dissolution process should be stirred. Then stand still, separate and remove the waste residue to obtain leachate, add phosphoric acid in the leachate to adjust the isoelectric point, obtain plant protein isolate, add shellac in the alkaline solution with a pH value of 10, the ratio of material to water is 1: 15, at temperature Dissolve under the condition of 29.5°C, the dissolution time is 100 minutes, the dissolution process should be stirred, and then stand still, separate and remove the waste residue to obtain the leachate, add phosphoric acid to the leachate, adjust the isoelectric point of the leachate to obtain animal protein isolation; separate the plant Protein and animal protein isolate are dissolved in a solution containing triethanolamine with a ...
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