Method for preparing efficient tilmicosin premixing agent through adsorption crystallization and application of efficient tilmicosin premixing agent
A technology of tilmicosin and tilmicosin phosphate, which is applied in the field of adsorption and crystallization to prepare high-efficiency tilmicosin premix, which can solve problems such as difficult crystallization, affecting use, and morphological changes of tilmicosin, so as to improve the taste , reduce drug side effects, improve selectivity and long-term feed intake
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Embodiment 1
[0035] This example provides a method for preparing high-efficiency tilmicosin premix by adsorption crystallization, including:
[0036] Adsorption and crystallization: spray the tilmicosin mixture into the porous material, boil and dry at 60°C for 13 minutes to obtain crystalline tilmicosin particles; the water content of the porous material is less than 1.5wt%, and the adsorption capacity of the porous material is less than 1.5 wt%. It is between 60 and 70%, the mesh number of the porous material is 45 mesh, and the porous material is corncob flour; the tilmicosin mixed solution includes tilmicosin, and the tilmicosin accounts for The weight percent of the tilmicosin mixture is 28wt%, the tilmicosin mixture also includes citric acid, and the citric acid accounts for 14wt% of the tilmicosin mixture, and the tilmicosin and the porous material The weight ratio is 1:1;
[0037] Coating: spraying the coating solution into the crystalline tilmicosin granules obtained after adsorp...
Embodiment 2
[0039] This example provides a method for preparing high-efficiency tilmicosin premix by adsorption crystallization, including:
[0040]Adsorption and crystallization: spray the tilmicosin mixture into the porous material, boil and dry at 70° C. for 10 min to obtain crystalline tilmicosin particles; the water content of the porous material is less than 1.5wt%, and the adsorption capacity of the porous material is less than 1.5 wt%. It is between 60 and 70%, the mesh number of the porous material is 60 mesh, and the porous material is corncob flour; the tilmicosin mixture includes tilmicosin, and the tilmicosin accounts for tilmicosin The weight percentage of the tilmicosin mixture is 35wt%, the tilmicosin mixture also includes phosphoric acid, and the phosphoric acid accounts for 20wt% of the tilmicosin mixture, and the weight of the tilmicosin and the porous material is 20% by weight. The ratio is 3:4;
[0041] Coating: spray the coating solution into the crystalline tilmico...
Embodiment 3
[0043] This example provides a method for preparing high-efficiency tilmicosin premix by adsorption crystallization, including:
[0044] Adsorption and crystallization: spray the tilmicosin mixture into the porous material, boil and dry at 55°C for 15 minutes to obtain crystalline tilmicosin particles; the water content of the porous material is less than 1.5wt%, and the adsorption capacity of the porous material is less than 1.5 wt%. It is between 60 and 70%, the mesh number of the porous material is 45 mesh, and the porous material is corncob flour; the tilmicosin mixed solution includes tilmicosin phosphate, and the tilmicosin phosphate is used The weight percentage of the micosin mixed solution is 40wt%, and the weight ratio of the total weight of the tilmicosin phosphate to the porous material is 1:1;
[0045] Coating: spraying the coating solution into the crystalline tilmicosin granules obtained after adsorption and crystallization, boiling and drying at 55° C. for 15 m...
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