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A kind of slurry for electronic grade glass fiber cloth and preparation method thereof

A glass fiber cloth and electronic grade technology, which is applied in the field of slurry for electronic grade glass fiber cloth and its preparation, can solve the problems of insufficient wear resistance and the desizing rate needs to be improved, so as to protect the surface from wear and promote the The effect of maintaining the suspended state and protecting the surface from damage

Active Publication Date: 2022-08-09
清远凯荣德电子专用材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the desizing rate needs to be improved, and the wear resistance of the first sizing is far from the wear resistance required for textiles, so a second sizing is still required

Method used

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  • A kind of slurry for electronic grade glass fiber cloth and preparation method thereof
  • A kind of slurry for electronic grade glass fiber cloth and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A slurry for electronic-grade glass fiber cloth, the raw material is composed of the following components: polyvinyl alcohol 1%, water-based rosin resin 0.08%, water-soluble phenolic resin 0.03%, tragacanth gum 0.5%, stabilizer 1%, lubricating agent 0.8%, the rest is deionized water.

[0033] The water-based rosin resin is composed of male rosin resin and acrylic modified rosin resin in a mass ratio of 12:1, and the stabilizer is a mixture of hypromellose and hydroxyethyl cellulose with a mass ratio of 1:0.5 ; Lubricant is sodium lauryl sulfate.

[0034] The preparation method of the slurry for electronic grade glass fiber cloth is as follows:

[0035] (1) Add polyvinyl alcohol, water-soluble phenolic resin, stabilizer and 50% lubricant to water and mix, heat to 55°C and stir for 30min;

[0036] (2) then add water-based rosin resin and tragacanth gum to (1) system, heat to 70 ℃ and stir for 30min;

[0037] (3) Finally, add the remaining lubricant and stir for 30min. ...

Embodiment 2

[0039] An electronic grade glass fiber cloth slurry, the raw material is composed of the following components: polyvinyl alcohol 0.5%, water-soluble rosin resin 0.1%, water-soluble phenolic resin 0.05%, tragacanth gum 0.2%, stabilizer 0.2%, Lubricant 0.2%, the rest is deionized water.

[0040] The water-based rosin resin is made up of male rosin resin and acrylic modified rosin in a mass ratio of 15:1; the stabilizer is a mixture of hypromellose and hydroxyethyl cellulose in a mass ratio of 1:1; The lubricant is sodium lauryl sulfate.

[0041] The preparation method of the slurry for electronic grade glass fiber cloth is as follows:

[0042] (1) Add polyvinyl alcohol, water-soluble phenolic resin, stabilizer and 50% lubricant to water and mix, heat to 60°C and stir for 20min;

[0043] (2) then add water-based rosin resin and tragacanth to the system (1), heat to 80°C and stir for 10min;

[0044] (3) Finally, add the remaining lubricant and stir for 20min.

Embodiment 3

[0046] An electronic grade glass fiber cloth slurry, the raw material is composed of the following components: polyvinyl alcohol 2%, water-soluble rosin resin 0.05%, water-based phenolic resin 0.01%, tragacanth gum 1.0%, stabilizer 2%, lubricating agent 0.8%, the rest is deionized water.

[0047] The water-based rosin resin is made up of male rosin resin and acrylic modified rosin resin in a mass ratio of 10:1: the stabilizer is a mixture of 1:0.5 hypromellose and hydroxyethyl cellulose; lubricant It is sodium lauryl sulfate.

[0048] The preparation method of the slurry for electronic grade glass fiber cloth is as follows:

[0049] (1) Add polyvinyl alcohol, water-soluble phenolic resin, stabilizer and 50% lubricant to the water and mix, heat to 50°C and stir for 20min;

[0050] (2) then add water-based rosin resin and tragacanth gum to (1) system, heat to 85 ℃ and stir for 20min;

[0051] (3) Finally, add the remaining lubricant and stir for 30min.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention belongs to the technical field of electronic glass fiber cloth, and particularly relates to a slurry for electronic-grade glass fiber cloth and a preparation method thereof. The raw materials of the slurry for electronic-grade glass fiber cloth include the following components: the raw materials of the slurry include 0.5-2% of polyvinyl alcohol, 0.05-0.1% of water-based rosin resin, 0.01-0.05% of water-based phenolic resin, and 0.1-1.0% of gum yarrow, 0.2-2% of stabilizer, 0.1-0.8% of lubricant, and the rest are deionized water. The preparation method is as follows: firstly, adding polyvinyl alcohol, water-based phenolic resin, stabilizer and some lubricants into water, mixing and stirring; then adding water-based rosin resin and tragacanth gum, stirring; finally adding remaining lubricant and stirring. The sizing provided by the invention has good adhesion and strong abrasion resistance, does not need secondary sizing before weaving, can protect the abrasion during the preparation of warp yarns, reduces the generation of broken silk and hairiness, and is easy to desizing.

Description

technical field [0001] The invention belongs to the technical field of electronic glass fiber cloth, and particularly relates to a slurry for electronic-grade glass fiber cloth and a preparation method thereof. Background technique [0002] Conductive fibers composited with resins such as carbon fiber, stainless steel, nickel fiber, etc. have been practically used, but they have not yet entered the stage of large-scale application due to price and performance constraints. Carbon black has excellent performance, but the price is relatively high; the ceramic matrix is ​​also limited in its application due to its brittleness. Carbon fiber has high temperature resistance, radiation resistance, good electrical conductivity, low density, and high specific strength, but the surface of carbon fiber is inert. Poor matrix adhesion. [0003] Glass fiber itself is an excellent inorganic non-metallic material with high mechanical properties, low price and excellent electrical insulation...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M15/333D06M15/17D06M15/41D06M15/09D06M15/03D06M13/262
CPCD06M15/333D06M15/17D06M15/41D06M15/03D06M15/09D06M13/262D06M2200/35D06M2200/40
Inventor 张国平
Owner 清远凯荣德电子专用材料有限公司
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