Activated carbon reactivation method
A technology of activated carbon and modification, applied in separation methods, chemical instruments and methods, inorganic chemistry, etc., to achieve the effect of ensuring connection effect, reducing material cost and ensuring stable performance
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Embodiment 1
[0019] A kind of active carbon resurrection method, comprises the steps:
[0020] Step 1, adding the modified nano glue into anhydrous ether and stirring evenly to obtain a slurry, the modified nano glue is titanium dioxide-based silicon oxide modified nano glue, the preparation method of the titanium dioxide-based silicon oxide modified nano glue, Including: a1, immerse the nano glue in water and ultrasonically wash for 10 minutes, then dry to obtain clean nano glue, the mass ratio of the nano glue to water is 2:7, the ultrasonic frequency of ultrasonic washing is 50kHz, and the drying temperature 120°C; a2, add ethyl silicate to anhydrous ether to form a silicon ether solution, then spray the silicon ether on the surface of the nanogel, dry it and leave it in the reaction kettle for 20 minutes, and dry it at a constant temperature to obtain a modified silicon oxide. Sexual nano glue, the concentration of said ethyl silicate in anhydrous ether is 40g / L, and the spray amount o...
Embodiment 2
[0027] A kind of active carbon resurrection method, comprises the steps:
[0028]Step 1, adding the modified nano glue into anhydrous ether and stirring evenly to obtain a slurry, the modified nano glue is titanium dioxide-based silicon oxide modified nano glue, the preparation method of the titanium dioxide-based silicon oxide modified nano glue, Including: a1, soaking the nano-glue in water for 20 minutes, and then drying to obtain clean nano-glue, the mass ratio of the nano-glue to water is 2:9, the ultrasonic frequency of ultrasonic washing is 80kHz, and the drying temperature is 150°C; a2, add ethyl silicate to anhydrous ether to form a silicon ether solution, then spray the silicon ether on the surface of the nanogel, dry it and leave it in the reaction kettle for 30 minutes, and dry it at a constant temperature to obtain a modified silicon oxide. Sexual nano glue, the concentration of said ethyl silicate in anhydrous ether is 100g / L, and the spray volume of said spray i...
Embodiment 3
[0035] A kind of active carbon resurrection method, comprises the steps:
[0036] Step 1, adding the modified nano glue into anhydrous ether and stirring evenly to obtain a slurry, the modified nano glue is titanium dioxide-based silicon oxide modified nano glue, the preparation method of the titanium dioxide-based silicon oxide modified nano glue, Including: a1, immerse the nano glue in water and ultrasonically wash for 15 minutes, then dry to obtain clean nano glue, the mass ratio of the nano glue to water is 2:8, the ultrasonic frequency of ultrasonic washing is 70kHz, and the drying temperature 140°C; a2, add ethyl silicate to anhydrous ether to form a silicon ether solution, then spray the silicon ether on the surface of the nanogel, dry it and leave it in the reaction kettle for 25 minutes, and dry it at a constant temperature to obtain a modified silicon oxide. Sexual nano glue, the concentration of described ethyl silicate in anhydrous ether is 80g / L, and the spray vol...
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