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Detection device and test method for determining gas containing soluble components

A technology of gas detection and testing method, which is applied in measuring devices, analyzing gas mixtures, analyzing materials, etc., can solve the problems of inability to guarantee an absolutely dry environment, it is difficult to ensure accurate measurement of ammonia gas, etc., and achieves low cost and simple operation. Effect

Pending Publication Date: 2022-01-11
SOUTHWEST PETROLEUM UNIV
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Problems solved by technology

[0002] When studying the modification effect of urea on heavy oil, it is necessary to mix urea solution with heavy oil, and then heat it in a high-temperature and high-pressure reactor. However, since the gas product contains ammonia gas which is very soluble in water, an absolutely dry environment cannot be guaranteed after the temperature is lowered, so it is difficult to ensure accurate measurement of ammonia gas

Method used

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  • Detection device and test method for determining gas containing soluble components
  • Detection device and test method for determining gas containing soluble components
  • Detection device and test method for determining gas containing soluble components

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Embodiment Construction

[0015] The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some, not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

[0016] see Figure 1~3 , in an embodiment of the present invention, a gas detection device and test method for determining soluble components, including a workbench, a water tank 6 is arranged on the workbench, and a gas separation device 7 is arranged in the water tank, and a high-temperature and high-pressure reaction kettle 5 is arranged on the left side of the water tank There is a high-precision pH tester 1 in front of the high-temperature and high-pressu...

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Abstract

The invention relates to the technical field of gas detection, discloses a detection device and a test method for determining gas containing soluble components, and aims to solve the problem that components and relative content of gas generated during modification need to be determined when a modification experiment of urea solution on thickened oil at high temperature and high pressure is studied, however, due to the fact that a gas product contains ammonia gas which is extremely soluble in water, the ammonia gas is difficult to accurately measure after the temperature is reduced, so that the ammonia gas is absorbed by introducing the gas into a cold water medium, the content of the ammonia gas in the gas is calculated by measuring the pH value, the content of the gas which is not absorbed is calculated by a separation device with scales, and finally, the relative content of the gas which is not absorbed is calculated by a mass spectrometer. According to the invention, cold water is used as an absorption medium, and mediums such as acid / alkaline, organic solvents and the like can also be used for pertinently absorbing gas which is not easy to detect through a gas detection device. And the device has wide application value.

Description

technical field [0001] The invention relates to the technical field of gas detection, in particular to a gas detection device and a test method for measuring easily soluble components. Background technique [0002] When studying the modification effect of urea on heavy oil, it is necessary to mix urea solution with heavy oil, and then heat it in a high-temperature and high-pressure reactor. The gas is collected, but since the gas product contains ammonia gas which is very soluble in water, an absolutely dry environment cannot be guaranteed after the temperature is lowered, so it is difficult to ensure accurate measurement of ammonia gas. [0003] Therefore, this patent separates ammonia from other gas components through a cold water medium, calculates the ammonia content of the gas through the measurement of the pH value, calculates the amount of gas through a separation device with a scale, and then measures the remaining gas through a mass spectrometer Relative content, s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N33/00G01N27/62
CPCG01N33/0004G01N27/62
Inventor 周翔何杰蒋琪于春生黄思源黄岢吴芳杰刘佳丽赵笑龚恒圆杨嗣民汪永朝
Owner SOUTHWEST PETROLEUM UNIV
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