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Detection method of spleen-enlivening capsule

A detection method and capsule technology, which are applied in measurement devices, instruments, scientific instruments, etc., can solve the problems of inability to effectively control the quality of the finished product of Xingpi capsule, small spot Rf value, tailing phenomenon, etc., and achieve the improvement of product quality inspection standards, Moderate Rf value and good spot separation

Pending Publication Date: 2021-10-26
贵州健兴药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Xingpi Capsules are recorded in WS-11534 (ZD-1534)-2002. The original testing items in the standard are: traits, microscopic identification, inspection, and extracts, but there are the following defects in the actual testing: (1) a little red thin For layer identification, the spots are small and fuzzy, the reproducibility is poor, and the Rf value of the spots is too small, which affects the judgment of the test results; (2) For the identification of the thin layer of gerbera, the main spots are blurred and have tailing phenomenon, and the Rf value of the spots is too small , the reproducibility is poor, which affects the judgment of the test results; (3) The detection method does not involve the TLC identification of spider incense, and cannot effectively control the quality of the finished product of Xingpi Capsules

Method used

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  • Detection method of spleen-enlivening capsule
  • Detection method of spleen-enlivening capsule
  • Detection method of spleen-enlivening capsule

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Embodiment 1 preparation method

[0031] [Prescription] A Little Red 395g, Hairy Gerbera 380g, Mountain Gardenia Tea 125g, Spider Fragrance 93g

[0032][Preparation method] Take 30g of the above four medicinal materials, crush them into fine powder, pass through an 80-mesh sieve for later use, soak the remaining three flavors such as a little red and gerbera in water for 30 minutes, decoct twice, the first time for 2 hours, and the second time After 1.5 hours, combine the decoction, filter, concentrate the filtrate to a clear paste with a relative density of 1.17-1.20 at 80°C, add a little red fine powder, mix well, dry, crush, pass through a 80-mesh sieve, add 10g of starch, mix Mix evenly, pack into capsules, make 1000 capsules, and get ready.

Embodiment 2

[0033] Embodiment 2 preparation method

[0034] [Prescription] A Little Red 395g, Hairy Gerbera 380g, Mountain Gardenia Tea 125g, Spider Fragrance 93g

[0035] [Preparation method] Take 30g of the above four medicinal materials, crush them into fine powder, pass through an 80-mesh sieve for later use, soak the remaining three flavors such as a little red and gerbera in water for 20 minutes, decoct twice, the first time for 1.5 hours, and the second time After 1 hour, combine the decoction, filter, concentrate the filtrate to a clear paste with a relative density of 1.17-1.20 at 80°C, add a little red fine powder, mix well, dry, pulverize, pass through a 80-mesh sieve, add 5g of starch, mix Mix evenly, pack into capsules, make 1000 capsules, and get ready;

Embodiment 3

[0036] Embodiment 3 preparation method

[0037] [Prescription] A Little Red 395g, Hairy Gerbera 380g, Mountain Gardenia Tea 125g, Spider Fragrance 93g

[0038] [Preparation method] Take 30g of the above four medicinal materials, crush them into fine powder, pass through an 80-mesh sieve for later use, soak the remaining three flavors such as a little red and gerbera in water for 40 minutes, decoct twice, the first time for 2.5 hours, and the second time After 2 hours, combine the decoction, filter, concentrate the filtrate to a clear paste with a relative density of 1.17-1.20 at 80°C, add a little red fine powder, mix well, dry, pulverize, pass through a 80-mesh sieve, add 15g of starch, mix Mix evenly, pack into capsules, make 1000 capsules, and get ready;

[0039] Detection method

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Abstract

The invention relates to a detection method of a spleen-enlivening capsule. The detection method comprises thin-layer identification of emilia sonchifolia, thin-layer identification of gerbera piloselloides and thin-layer identification of valeriana jatamansi jones in the capsule. According to the detection method, thin-layer identification of a valeriana jatamansi jones medicinal material is added on the basis of an original detection method, a thin-layer identification method of emilia sonchifolia and gerbera piloselloides medicinal materials is optimized, methodological investigation shows that the detection method has the effects that specificity is high, durability is good, spots are clear after thin layers are expanded, the separation degree meets the requirement, and the Rf value is moderate; and the product quality condition can be effectively controlled, the product quality detection standard is improved, and the product quality is guaranteed.

Description

technical field [0001] The invention relates to the field of drug detection, in particular to a detection method for Xingpi capsules. Background technique [0002] Xingpi Capsule, a product of Guizhou Jianxing Pharmaceutical Co., Ltd., is a Chinese patent medicine preparation, which has the effects of refreshing the spleen and appetizing, nourishing blood and calming the nerves, strengthening the intestines and stopping diarrhea, and is effective in treating symptoms such as restless sleep at night and loss of appetite caused by spleen deficiency. better. [0003] Xingpi Capsules are recorded in WS-11534 (ZD-1534)-2002. The original testing items in the standard are: traits, microscopic identification, inspection, and extracts, but there are the following defects in actual testing: (1) Thin For layer identification, the spots are small and fuzzy, the reproducibility is poor, and the Rf value of the spots is too small, which affects the judgment of the test results; (2) For ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 孙小鹦廖萍廖伟廖忠
Owner 贵州健兴药业有限公司
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