Vulcanization composition based on nitrile rubber, vulcanized rubber and preparation method and application thereof
A nitrile rubber and composition technology, applied in the field of rubber, can solve problems such as the matching of rubber sealing material processing technology and product performance, and achieve excellent mechanical properties, compression set resistance, and good processing performance. Effect
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Embodiment 1
[0079] The composition formula of this embodiment is shown in Table 2.
[0080] The preparation method of vulcanized rubber is as follows:
[0081] First mixing:
[0082] Set the initial temperature of the internal mixer to 70°C and the rotational speed to 70rpm, add the rubber matrix, reinforcing agent, calcium sulfate whisker, vulcanization activator, anti-aging agent and plasticizer into the internal mixer for the first mixing for 4 minutes, and deglue , parked for 4h to obtain the masterbatch.
[0083] Second mixing:
[0084] Set the initial temperature of the internal mixer to 50°C, and the rotational speed to 60 rpm, put the masterbatch, vulcanizing agent and vulcanization accelerator into the internal mixer, mix for 3 minutes, and discharge the rubber.
[0085] Pass the rubber compound obtained by the above method once on the open mill with a roller distance of 0.5mm and a roller temperature of 60±5°C, then adjust the roller distance to 5mm, and pass it twice, and pa...
Embodiment 10
[0088] The composition formulation of the present embodiment is exactly the same as that in Example 1.
[0089] The preparation method of vulcanized rubber is as follows:
[0090] Set the initial temperature of the internal mixer to 55°C and the rotational speed to 60rpm, add the rubber matrix, reinforcing agent, calcium sulfate whisker, vulcanization activator, anti-aging agent and plasticizer into the internal mixer and mix for 4 minutes, lift the internal mixer to the top Put the masterbatch, vulcanizing agent and vulcanization accelerator into the internal mixer, drop the top bolt on the internal mixer, continue mixing for 3 minutes, and discharge the glue. Pass the rubber compound obtained by the above method once on the open mill with a roller distance of 0.5mm and a roller temperature of 60±5°C, then adjust the roller distance to 5mm, and pass it twice, and park the obtained mixed rubber for 24h.
[0091] The above mixed rubber was pressed into tablets in an open mill,...
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