Tracheostomy tube body and preparation process thereof
A tracheotomy and intubation technology, applied in the field of tracheotomy intubation tube body and its preparation, can solve the problems of comfort of mucous membrane injury in the trachea, high tube body hardness, water loss, etc. Guaranteed flexibility and low Shore hardness
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preparation example 1
[0060] A kind of modified polyvinyl chloride, its preparation steps are as follows:
[0061] a. Modification treatment: first mix polyvinyl chloride resin, modified emulsion and initiator in a weight ratio of 1:0.1:0.005, that is, stir at 80°C for 5min at a speed of 80r / min, and then heat up to 180°C °C, under vacuum conditions, at a speed of 200r / min, stir for 4h to prepare the modified material;
[0062] The modified emulsion is composed of tributyl citrate, tetramethyltetravinylcyclotetrasiloxane, and octamethylcyclotetrasiloxane in a weight ratio of 1: 0.01:1;
[0063] The initiator is sodium trimethylsilanolate;
[0064] b. Softening treatment: Mix the modified material, lubricant and surfactant in a weight ratio of 1:0.1:0.05, that is, stir at a speed of 80r / min for 1h at 80°C to obtain a modified polychloride vinyl.
[0065] The lubricant is calcium stearate;
[0066] The surfactant is coconut acid diethanolamide.
preparation example 2
[0068] A modified polyvinyl chloride, the difference from Preparation Example 1 is that the preparation steps are as follows:
[0069] a. Modification treatment: Stir the polyvinyl chloride resin, modified emulsion and initiator at 90°C at a speed of 80r / min for 7.5min, then raise the temperature to 190°C, and stir at 200r / min under vacuum. The rotating speed, stir 4.5h, make modified material;
[0070] b. Softening treatment: Stir the modified material, lubricant and surfactant at 90°C at a speed of 80r / min for 1.5h to prepare modified polyvinyl chloride.
preparation example 3
[0072] A modified polyvinyl chloride, the difference from Preparation Example 1 is that the preparation steps are as follows:
[0073] a. Modification treatment: Stir the polyvinyl chloride resin, modified emulsion and initiator at a speed of 80r / min for 10min at 100°C, then raise the temperature to 200°C, and stir at a speed of 200r / min under vacuum. Rotating speed, stirring for 5h, obtained modified material;
[0074] b. Softening treatment: Stir the modified material, lubricant and surfactant at 100°C for 2 hours at a speed of 80r / min to obtain modified polyvinyl chloride.
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Abstract
Description
Claims
Application Information
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