Hydrate sediment in-situ permeability pressure gradient and mechanical property measuring system

A technology of hydrate deposits and pressure gradients, applied in permeability/surface area analysis, measuring devices, scientific instruments, etc., can solve problems such as hindering CT shooting, specific analysis cannot be observed and studied, and pressure changes and hydrate formation areas are difficult to implement. , to achieve the effect of reducing the occlusion problem

Active Publication Date: 2020-11-24
CHINA NAT OFFSHORE OIL CORP +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1. At this stage, the device for simulating and measuring the internal permeability pressure of the sample can only study the approximate pressure of the entire sample, and it is difficult to characterize the pressure change of the sample at each position in the simulated environment and the corresponding hydrate formation area;
[0005] 2. For the research on the mechanical failure performance of hydrate under axial pressure, the current research can only study the macroscopic mechanical properties, and there is no way to observe and study the specific analysis at the microscopic level;
[0006] 3. The confining pressure of liquid silicone oil and the cooling of the water bath wrapping the reactor in the experimental device greatly hinder the clarity of CT shooting, and cannot be used for CT microscopic research;
[0007] 4. The exterior material used in the pressure chamber is pure aluminum or aluminum alloy and other low-density materials with good thermal conductivity, which is easy to cause heat loss and affect the temperature change during the experiment, and the water bath is still distributed around the pressure chamber, which hinders CT shooting. And it is impossible to study the change of permeability pressure at the micro level

Method used

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  • Hydrate sediment in-situ permeability pressure gradient and mechanical property measuring system
  • Hydrate sediment in-situ permeability pressure gradient and mechanical property measuring system

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Experimental program
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Effect test

Embodiment 1

[0030] Such as figure 1 , figure 2As shown, the present invention provides a system for measuring in-situ permeability pressure gradient and mechanical properties of hydrate deposits, which includes: reaction kettle, sediment sample 5, confining pressure loading device, pore pressure loading device, axial pressure loading device, refrigeration device, data acquisition device and control display 31. Specifically, the reaction kettle includes a base, a pressure chamber main body 14 and an upper end cover 8 . Wherein, the pressure chamber main body 14 adopts a hollow "I"-shaped structure, and the middle parts of the upper and lower ends of the pressure chamber main body 14 are respectively provided with a first cylindrical groove whose diameter is larger than the hollow part, and the two first cylindrical grooves There is no communication with the hollow part of the pressure chamber main body 14; the base includes a bottom base 2 and a base substrate 16 connected by a connecti...

Embodiment 2

[0042] When using the above-mentioned in-situ permeability pressure gradient and mechanical property measurement system for hydrate deposits to measure the mechanical properties of hydrate deposits, the following steps are included:

[0043] (1) Connecting pipeline: the device of the present invention is placed on the CT equipment stage, and according to figure 2 As shown, the reaction kettle is respectively connected with the confining pressure loading device, the pore pressure loading device, the axial pressure loading device, the refrigeration device and the data acquisition device.

[0044] The specific connection method is:

[0045] Confining pressure loading device: connect one end of the confining pressure air intake line to the confining pressure air inlet provided at the lower part of the pressure chamber main body 14, and connect the other end to the confining pressure loading pump 18, needle valve 19(a) and nitrogen cylinder 20 in sequence, and the nitrogen cylinde...

Embodiment 3

[0057] When the above gas hydrate deposit in-situ permeability pressure and mechanical property measurement system is used to measure the mechanical properties, specifically, the following steps are included:

[0058] (1)-(6): The process is consistent with the steps (1)-(6) in the second embodiment.

[0059] (7) Osmotic pressure measurement stage: the experiment is measured by the constant pressure method. After the consolidation is completed, the pore pressure loading pump 24 is adjusted to a stable pressure of 10 MPa, and the pressure of the back pressure valve 28 at the gas outlet of the pore pressure is adjusted to 6 MPa. During the sampling process, the flow rate and flow rate change until the final flow rate of the gas flow meter 30 remains at a constant value, and the flow rate and pressure are brought into the permeability formula to obtain the permeability value, and at the same time, the pressure at different positions in the permeation process is observed.

[0060]...

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Abstract

The invention relates to a hydrate sediment in-situ permeability pressure gradient and mechanical property measuring system. The system comprises a reaction kettle, a sediment sample, a confining pressure loading device, a pore pressure loading device, an axial pressure loading device, a refrigerating device, a data acquisition device and a control display, the reaction kettle is used for containing a sediment sample and is connected with other devices; the axial pressure loading device is used for loading axial pressure to the sediment sample through an axial loading piston; the pore pressureloading device is used for applying pore pressure to the sediment sample; the confining pressure loading device is used for applying confining pressure to a confining pressure chamber; the refrigerating device is used for controlling the temperature of the sediment sample; the data acquisition device is used for acquiring temperature and pressure data of the sediment sample in the experiment process; and the control display is used for controlling the axial pressure loading device and the refrigerating device and processing and displaying data acquired by the data acquisition device. The system can be widely applied to the field of hydrate measurement.

Description

technical field [0001] The invention relates to a measurement system for in-situ permeability pressure gradient and mechanical properties of hydrate deposits suitable for CT, belonging to the field of geotechnical engineering basic physical property measurement. Background technique [0002] Hydrate, as a new energy source with huge reserves, high energy density, and clean and pollution-free, has successfully attracted the attention of people all over the world. A series of geological disasters such as landslides and wellbore instability. Therefore, it is necessary to study the permeability pressure change at the microscopic level and its mechanical properties at the macroscopic level. [0003] However, there are many problems in the current research: [0004] 1. At this stage, the device for simulating and measuring the internal permeability pressure of the sample can only study the approximate pressure of the entire sample, and it is difficult to characterize the pressur...

Claims

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Application Information

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IPC IPC(8): G01N15/08G01N23/046
CPCG01N15/0826G01N23/046Y02A90/30
Inventor 李清平宋永臣庞维新吕鑫黄婷杨明军李洋辉葛阳樊奇周云健王清朱军龙赵晶瑞
Owner CHINA NAT OFFSHORE OIL CORP
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