Method for preparing electrochemical nano dot array electrode by using ultra-long nanowire
A nano-dot array and nano-wire array technology, applied in the direction of material electrochemical variables, nanotechnology for sensing, nanotechnology, etc., can solve the problems of high cost of processing equipment, poor size controllability, complicated process, etc. Achieve the effects of low processing cost, controllable size and shape, and simple instrument operation
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specific Embodiment approach 1
[0024] Specific implementation mode 1: This implementation mode records a method for preparing an electrochemical nano-dot array electrode by using ultra-long nanowires, and the steps of the method are:
[0025] Step 1: Pouring PDMS on a commercial silicon template containing micron groove arrays;
[0026] Step 2: pouring resin on the cured PDMS mold to obtain a resin block with a micron groove array;
[0027] Step 3: Deposit a layer of metal film on the resin block to obtain a metal-resin composite structure;
[0028] Step 4: Embedding the composite structure obtained in Step 3 with resin to obtain a resin-metal-resin embedding block;
[0029] Step 5: Nano-slicing the embedding block obtained in Step 4 to obtain a resin sheet containing a nanowire array;
[0030] Step 6: transferring the single resin sheet containing nanowire arrays obtained in step 5 or multiple resin sheets containing nanowire arrays alternately stacked with empty resin sheets to a substrate to obtain a n...
specific Embodiment approach 2
[0033] Embodiment 2: In Embodiment 1, a method for preparing electrochemical nano-dot array electrodes by using ultra-long nanowires, in step 1, the metal thin film has a thickness of 2 nm to 1 μm.
specific Embodiment approach 3
[0034] Embodiment 3: In Embodiment 1 or 2, a method for preparing electrochemical nano-dot array electrodes by using ultra-long nanowires, in step 1, the metal is one of gold, platinum or silver.
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