Preparation of plant essential oil microcapsule and application of the plant essential oil microcapsule in hair product with long-lasting fragrance
A technology of plant essential oils and microcapsules, which is applied to medical preparations, toiletry preparations, and cosmetic preparations containing active ingredients, and can solve problems such as difficulty in maintaining the integrity and stability of plant essential oil inclusion complexes for a long time. Achieve long-term moisturizing scalp and hair, small microcapsule particle size, and improved formula stability
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Embodiment 1
[0044] Embodiment 1: the preparation of plant essential oil microcapsule
[0045] (1) First weigh β-cyclodextrin and add it to hot water at 80±5°C, stir and dissolve to make a cyclodextrin saturated solution;
[0046] (2) add water and make the saturated solution temperature of step (1) drop to 35 ± 5 ℃ when still be saturated solution, then add the ethanol solution that concentration is the marigold essential oil of 10wt% in cyclodextrin saturated solution, wherein the plant essential oil The mass ratio of the plant essential oil in the ethanol solution to the cyclodextrin in the cyclodextrin saturated solution is 1:2, stir at 60°C for 2h, then refrigerate at 0°C for 24h, then take it out, centrifuge, and wash the obtained solid repeatedly with absolute ethanol, Then freeze-dry the solid at -10°C for 24 hours to obtain the cyclodextrin inclusion compound of plant essential oil;
[0047] (3) Mix and stir the cyclodextrin inclusion compound of the above-mentioned plant essenti...
Embodiment 2~4
[0052] Embodiment 2~4: the preparation of the shampoo containing plant essential oil microcapsules
[0053] The formula of the shampoo containing plant essential oil microcapsules in Examples 2 to 4 is shown in Table 1 below. In order to highlight the effect of plant essential oil microcapsules in the present invention, two groups of comparative examples 1 to 2 are set, wherein comparative examples 1 to 2 In 2, instead of adding plant essential oil microcapsules, add plant essential oil, and the specific formula is as shown in Table 1 below;
[0054] The formula of shampoo in table 1 embodiment 2~4 and comparative example 1~2
[0055]
[0056] The preparation steps of the hair shampoo in Examples 2~4 and Comparative Examples 1~2 are as follows:
[0057] (1) Put pure water accounting for 60% of the total amount of water into a container that can be heated and stirred, turn on the heating and stirring at a heating temperature of 50°C, and then add polyquaternium-10 to it;
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