Multi-component photoinitiating system and photopolymer material

A photopolymer, light-induced technology, applied in the field of photosensitive materials, can solve the problems of monotonous two-dimensional information display, storage density close to the theoretical limit, and insufficient image information display.

Active Publication Date: 2021-07-06
BEIHANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] Today's world is in the era of informationization, and various high-tech industries have higher and higher requirements for information storage, and the storage technologies widely used at present are all surface storage technologies, such as magnetic storage or optical disk storage, and the storage density is close to the theoretical level. In addition, the two-dimensional information display method has become somewhat monotonous, and the display of image information is not comprehensive enough. The true three-dimensional and immersive information display method has become the focus of attention. Therefore, the research on the new storage technology of the whole series storage imperative

Method used

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  • Multi-component photoinitiating system and photopolymer material
  • Multi-component photoinitiating system and photopolymer material
  • Multi-component photoinitiating system and photopolymer material

Examples

Experimental program
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Effect test

Embodiment 1

[0040] Step 1: Preparation of solvent-based photopolymer photosensitive liquid

[0041]Under a red safe light, according to the order of the method for preparing photopolymer materials involved in the present invention, film-forming agent PVAc 69.8wt%, photosensitizer BDMA 0.4wt%, nitrogen-containing condensed heterocyclic compound MBO with mercapto 2wt%, photoinitiator TCDM-HABI 8.8wt%, monomer POEA 8wt%, plasticizer tricresyl phosphate 11wt% dissolved in solvent DMF, and configured as a solvent-based photopolymer photosensitive liquid with a content of 15wt%.

[0042] Step 2: Preparation of solvent-based photopolymer film

[0043] Under the red safe light environment, take an appropriate amount of solvent-based photopolymer photosensitive liquid, apply it on the clean glass surface by drop coating, and dry it under heating at 40°C in the dark to obtain a final thickness of 60 μm. photopolymer films.

Embodiment 2

[0045] Step 1: Preparation of solvent-based photopolymer photosensitive liquid

[0046] Under the red safe lamp, according to the order of the method for preparing photopolymer material involved in the present invention, film-forming agent PVAc 77.5wt%, photosensitizer BDEA 0.5wt%, nitrogen-containing condensed heterocyclic compound MBO with mercapto 2.5wt%, photoinitiator o-Cl-HABI 10.3wt%, monomer POEA 9wt%, fluorosurfactant FC-4430 0.2% used as a leveling agent dissolved in the solvent DMF, configured to a content of 15wt% Solvent-based photopolymer photosensitive fluid.

[0047] Step 2: Preparation of solvent-based photopolymer film

[0048] Under the red safe light environment, take an appropriate amount of solvent-based photopolymer photosensitive liquid, apply it on the clean glass surface by drop coating, and dry it under heating at 40°C in the dark to obtain a final thickness of 60 μm. photopolymer films.

Embodiment 3

[0050] Step 1: Preparation of solvent-based photopolymer photosensitive liquid

[0051] Under the red safe light, according to the order of the method for preparing photopolymer material involved in the present invention, film-forming agent PVAc 77.5wt%, photosensitizer BDEA 0.5wt%, nitrogen-containing condensed heterocyclic compound MBI with mercapto 2.5wt%, photoinitiator o-Cl-HABI 10.5wt%, and monomer POEA 9wt% were dissolved in the solvent DMF to form a solvent-based photopolymer photosensitive liquid with a content of 15wt%.

[0052] Step 2: Preparation of solvent-based photopolymer film

[0053] Under the red safe light environment, take an appropriate amount of solvent-based photopolymer photosensitive liquid, apply it on the clean glass surface by drop coating, and dry it under heating at 40°C in the dark to obtain a final thickness of 60 μm. photopolymer films.

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Abstract

A multi-component photoinitiation system and a photopolymer material, the multi-component photoinitiation system includes a photoinitiation accelerator of the structure shown in formula (1): wherein, X is O, S or N, and R is selected from H, halogen or nitro. Applying the multi-component photoinitiating system to the photopolymer material can significantly improve the performance of the photopolymer.

Description

technical field [0001] The invention relates to the technical field of photosensitive materials, in particular to a multi-component photoinitiating system and a photopolymer material. Background technique [0002] Today's world is in the era of informationization, and various high-tech industries have higher and higher requirements for information storage, and the storage technologies widely used at present are all surface storage technologies, such as magnetic storage or optical disk storage, and the storage density is close to the theoretical level. In addition, the two-dimensional information display method has become a little monotonous, and the image information display is not comprehensive enough. The true three-dimensional and immersive information display method has become the focus of attention. Therefore, the research on this new storage technology of the whole system It is imperative. As a class of holographic storage materials, photopolymers have the characteris...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F2/48G03F7/027G03F7/004
CPCC08F2/48G03F7/004G03F7/027
Inventor 李卫平史志伟陈海宁刘慧丛
Owner BEIHANG UNIV
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