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Smokeless sulfur-free magenta indoor setting-off type cold firework agent and preparation method thereof

A cold fireworks and discharge type technology, applied in explosives processing equipment, explosives, offensive equipment and other directions, can solve problems such as environmental pollution, audience disgust, impact on human health, etc., and achieves simple process, few steps, and significant economic and social benefits. Effect

Inactive Publication Date: 2020-04-10
BEIJING INSTITUTE OF TECHNOLOGYGY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its discharge will produce chloride and sulfide smoke and metal oxide dust, which will affect human health and cause certain pollution to the environment; When the color is not bright or there are residues, it will arouse the disgust of the audience, and the effect of celebration and the purpose of adding color will not be achieved.
Moreover, the lack of effective formulas and preparation methods for magenta cold smoke flower medicaments on the market is a weak area for the preparation of cold smoke flower medicaments, and also limits the application diversity of cold smoke flower medicaments

Method used

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  • Smokeless sulfur-free magenta indoor setting-off type cold firework agent and preparation method thereof
  • Smokeless sulfur-free magenta indoor setting-off type cold firework agent and preparation method thereof
  • Smokeless sulfur-free magenta indoor setting-off type cold firework agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A kind of smokeless and sulfur-free magenta indoor discharge type cold smoke flower agent, its components and their mass percentages are as follows:

[0037]

[0038] The nitrogen content of the nitrobamboo cellulose in the components is 12% to 12.5%;

[0039] Add 200g of nitrobamboo cellulose to 1000g of ethyl acetate, stir the above mixed solution at a rate of 60rpm, add 70g of aluminum stearate and 30g of melamine under stirring, and stir for 30 minutes to prepare solution A;

[0040] Use a steel brush to remove the oxide layer on the surface of the zirconium ingot, place the zirconium ingot in an ultrasonic cleaner, and clean it with absolute ethanol. After cleaning for 15 minutes, place the zirconium ingot at 40°C for 5 minutes in vacuum, and then Weigh 160g of zirconium ingot; place 160g of zirconium ingot, 290g of light producing agent and 350g of light aid on the bottom of the crucible of the vacuum induction furnace, seal the vacuum induction furnace, turn o...

Embodiment 2

[0050] A kind of smokeless and sulfur-free magenta indoor discharge type cold smoke flower agent, its components and their mass percentages are as follows:

[0051]

[0052] The nitrogen content of the nitrobamboo cellulose in the components is 12% to 12.5%;

[0053] Add 1.7kg of nitrobamboo cellulose to 10.2kg of ethyl acetate, stir the above mixed solution at a rate of 70rpm, add 0.5kg of aluminum stearate and 0.3kg of melamine under stirring, and stir for 30 minutes to obtain Solution A;

[0054] Use a steel brush to remove the oxide layer on the surface of the zirconium ingot, place the zirconium ingot in an ultrasonic cleaner, and clean it with absolute ethanol. After cleaning for 15 minutes, place the zirconium ingot at 40°C for 5 minutes in vacuum, and then Weigh 1.7kg of zirconium ingot; place 1.7kg of zirconium ingot, 3.6kg of luminescence agent and 3.2kg of light aid on the bottom of the crucible of the vacuum induction furnace, seal the vacuum induction furnace,...

Embodiment 3

[0064] A kind of smokeless and sulfur-free magenta indoor discharge type cold smoke flower agent, its components and their mass percentages are as follows:

[0065]

[0066] The nitrogen content of the nitrobamboo cellulose in the components is 12% to 12.5%;

[0067] Add 2.5kg of nitrobamboo cellulose to 13kg of ethyl acetate, stir the above mixed solution at a rate of 100rpm, add 0.5kg of aluminum stearate and 0.5kg of melamine under stirring, and stir for 40 minutes to obtain a solution A;

[0068] Use a steel brush to remove the oxide layer on the surface of the titanium ingot, place the titanium ingot in an ultrasonic cleaner, and clean it with absolute ethanol. After cleaning for 15 minutes, place the titanium ingot at 40°C for 5 minutes in vacuum, and then Weigh 1.8kg of titanium ingot; place 1.8kg of titanium ingot, 3.6kg of luminescence agent and 1.8kg of light aid on the bottom of the crucible of the vacuum induction furnace, seal the vacuum induction furnace, and...

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Abstract

The invention relates to a smokeless sulfur-free magenta indoor setting-off type cold firework agent and a preparation method thereof, and belongs to the field of environment-friendly pyrotechnic compositions. The preparation method comprises the steps: weighing the modified alloy type flame retardant, the nitrocellulose, the aluminum stearate and the melamine; adding the nitrified bamboo cellulose into ethyl acetate, stirring and adding the aluminum stearate and the melamine to obtain a solution A; and adding the modified magenta flame coloring agent into the solution A, stirring, drying andkneading to form uniform micelles with moderate hardness, granulating, drying to obtain a smoke-free sulfur-free magenta indoor setting-off type cold firework agent crude product, crushing and sievingto obtain the smoke-free sulfur-free magenta indoor setting-off type cold firework agent with uniform particles. The method is safe and reliable and no toxic or harmful smoke is generated; the preparation method has the advantages of simple process, few steps and no emission of three wastes in the production process.

Description

technical field [0001] The invention relates to a smokeless and sulfur-free magenta indoor discharge type cold smoke flower agent and a preparation method thereof, belonging to the field of environment-friendly pyrotechnic agents. Background technique [0002] The development of cold fireworks marks that the fireworks industry is moving towards a new stage. Its advantages such as environmental protection and low discharge temperature are new trends in the future development of the fireworks industry and have strong competitiveness in the market. [0003] Patent CN108218644A discloses a smokeless and scented luminescent fireworks agent. The components of the luminescent fireworks agent include: nitrocellulose, ferrocene, stabilizer, essence, and titanium powder. By adjusting the ratio of each component, the luminescent fireworks agent The ideal eruption effect is achieved, but the color of the luminescent fireworks agent disclosed in this patent is single during the discharge...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C06B33/08C06B21/00
CPCC06B21/0066C06B33/08
Inventor 刘吉平方祝青李雪利于保藏李琪军刘克普吉伟生周耀明
Owner BEIJING INSTITUTE OF TECHNOLOGYGY
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