Extraction method of alpinia galanga rhizome flavonoids
A technology of galangalone and an extraction method, which is applied in the field of extraction of galangaloid compounds, can solve the problems of waste of resources, less flavonoids, low extraction yield and purity of flavonoids, etc., and achieves the effects of reducing waste and improving extraction rate.
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Embodiment 1
[0031] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:
[0032] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water and grind it to obtain galangal juice; the mass ratio of galangal to purified water is 1:1.5 ; The grinding is to grind Galangal to cross 80 mesh sieves;
[0033] (2) Microwave extraction: microwave extraction is carried out to the southern ginger juice obtained in step (1), repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.1KHz, power is 400W, and stirring speed is 20r / min, the time is 25min;
[0034](3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the extract obt...
Embodiment 2
[0038] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:
[0039] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water for grinding, and obtain galangal juice; the mass ratio of galangal to purified water=1:2 ; The grinding is to grind Galangal to cross 100 mesh sieves;
[0040] (2) Microwave extraction: microwave extraction is carried out to the southern ginger pulp juice that step (1) obtains, repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.2KHz, and power is 450W, and stirring speed is 25r / min, the time is 30min;
[0041] (3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the ex...
Embodiment 3
[0045] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:
[0046] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water and grind it to obtain galangal juice; the mass ratio of galangal to purified water is 1:1.6 ; The grinding is to grind Galangal to cross 85 mesh sieves;
[0047] (2) Microwave extraction: microwave extraction is carried out to the southern ginger pulp juice that step (1) obtains, repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.12KHz, and power is 410W, and stirring speed is 21r / min, the time is 26min;
[0048] (3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the...
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