Chitosan microsphere loaded nano silver antibacterial polypropylene material, composite antibacterial agent and preparation method thereof
A technology of chitosan microspheres and composite antibacterial agent is applied in the field of composite antibacterial agent and its preparation. Chitosan microspheres are loaded with nano-silver antibacterial polypropylene material, which can solve the problems of high surface energy and large specific surface area, etc. Good compatibility, simple preparation process and cost reduction effect
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Embodiment 1
[0032] A chitosan microsphere-loaded nano-silver antibacterial polypropylene material, the raw material composition comprises polypropylene resin and homemade chitosan microsphere / nano-silver composite antibacterial agent, wherein the polypropylene resin is 100 parts by weight, and the composite antibacterial agent 8 parts; the composite antibacterial agent uses chitosan microspheres as a carrier, and nano-silver is loaded on the chitosan microspheres, and the mass ratio of nano-silver to chitosan is 5 / 100.
[0033] The preparation method of described chitosan microsphere / nano-silver composite antibacterial agent is:
[0034](1) Preparation of chitosan microspheres: Dissolve 100 mg chitosan powder in 50 mL acetic acid solution with a volume concentration (v / v) of 1% at room temperature, keep stirring until completely dissolved, and then wash with NaOH The pH value of the solution adjustment system was 5. Keep the state of magnetic stirring, use a syringe to draw 20 mL of sodi...
Embodiment 2
[0039] Except that the anionic gelling agent in the preparation step (1) of the chitosan microsphere / nano-silver composite antibacterial agent was adjusted to 20 mL of sodium tetrapolyphosphate solution with a concentration of 1 mg / mL, other process steps were the same as in Example 1 .
Embodiment 3
[0041] Except that the anionic surfactant in the step (2) of preparing the chitosan microsphere / nano-silver composite antibacterial agent was adjusted to 13.3 mg sodium lauryl sulfate, other process steps were the same as in Example 1.
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