Nano cuprous oxide/silk fibroin complex and preparation method thereof
A technology of nano-cuprous oxide and silk fibroin, applied in the field of nano-materials, can solve problems such as affecting performance, uneven dispersion of cuprous oxide, easy oxidation of cuprous oxide, etc., achieving low cost, easy industrial production, strong The effect of applying value
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0028] First add 100 grams of cocoons to 1 liter of 0.5w / v% Na 2 CO 3 In the aqueous solution, boil for 30min, repeat the treatment three times, fully wash with distilled water, put it in a drying oven at 45°C after washing, and dry to obtain degummed silk fibers; 2 :C 2 h 5 OH:H 2 The molar ratio of O=1:2:8 is used to prepare a ternary solvent, and the silk fiber is hydrolyzed at a constant temperature in a water bath at 70° C. for 1 hour at a bath ratio of 1:10 to obtain a completely dissolved brownish-yellow silk fiber hydrolysis solution; Put the hydrolyzed solution into a dialysis bag, dialyze with distilled water for 72 hours, put the dialyzed silk fiber hydrolyzed solution into -80°C for 12 hours, and then freeze-dry it at -58°C until dry to obtain white, loose porous, spongy Silk fibroin: Compared with the existing commercially available silk fibroin, the silk fibroin prepared by the above steps of the present invention has the advantages of uniform molecular weigh...
Embodiment 2
[0038] Add 0.2g silk fibroin to 10mL water and stir until completely dissolved to obtain a silk fibroin solution; add 0.08mol.L -1 Add 10mL of copper sulfate solution to the silk fibroin solution and stir evenly, add 0.2mol.L -1 Sodium hydroxide to adjust the pH value to 12, add 0.08mol.L -1 Take 20 mL of vitamin C solution, react at room temperature (25° C.) for 48 hours, dialyze for 3 days, and freeze-dry to obtain nano-cuprous oxide / silk fibroin complex.
Embodiment 3
[0040] Add 0.2g silk fibroin to 10mL water and stir until completely dissolved to obtain a silk fibroin solution. Add 0.04mol.L -1 Add 10mL of copper sulfate solution to the silk fibroin solution and stir evenly, add 0.2mol.L -1 Sodium hydroxide to adjust the pH value to 12, add 0.08mol.L -1 Vitamin C solution, 20mL, reacted at room temperature (25°C) for 48 hours, dialyzed for 3 days, and freeze-dried to obtain nano-cuprous oxide / silk fibroin complex.
[0041] Table 1 below shows the contents of nitrogen, oxygen, carbon and copper elements in the nano-cuprous oxide / silk fibroin composite prepared in different examples from X-ray photoelectron spectroscopy (XPS).
[0042] Table 1 Contents of nitrogen, oxygen, carbon and copper elements in the nano-cuprous oxide / silk fibroin composites prepared in different examples.
[0043] Table 1
[0044]
[0045] The data in the above table shows that with the increase of the concentration of copper sulfate, the content of copper ele...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com