AC33/nano calcium hydroxide containing organic inorganic composite material for reinforcing ancient murals and reinforcing method
An inorganic composite material, calcium hydroxide technology, applied in pigmented coatings, paper coatings, preserved paintings, etc., can solve the problems of slow action, low reinforcement efficiency, low reinforcement strength, etc., to overcome slow action and low cost Low cost, simple preparation method and time-saving effect
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[0017] The invention provides an organic-inorganic composite material containing AC33 / nano-calcium hydroxide for reinforcement of ancient murals and a preparation method thereof, wherein the mass ratio of AC33 and nano-calcium hydroxide is adjustable within the range of 5:1-1:1 , and the rest is ethyl acetate solution: it is mainly prepared by the following steps:
[0018] Step 1, the preparation of the organic-inorganic composite material containing AC33 / nano-calcium hydroxide: take commercially available AC33 solid and nano-calcium hydroxide powder and mix so that the mass ratio is 5:1-1:1, wherein the nano-calcium hydroxide The preparation refers to our patent: Chinese patent, patent number, 201711361358.7. Dissolving the mixture of AC33 solid and nano calcium hydroxide powder in ethyl acetate solution to form a solution with a mass fraction of 1%-8% is prepared to prepare an organic-inorganic composite material containing AC33 / nano calcium hydroxide.
[0019] Step 2, the ...
Embodiment 1
[0021] Weigh the commercially available AC33 solid and nano-calcium hydroxide powder and mix to make the mass ratio 5:1. The preparation of nano-calcium hydroxide refers to our patent: Chinese patent, patent number, 201711361358.7. The mixture of AC33 solid and nanometer calcium hydroxide powder is dissolved in ethyl acetate solution to form a mass fraction of 1%, 2%, 3%, 4%, and 5% to prepare an organic-inorganic composite containing AC33 / nanometer calcium hydroxide Material.
[0022] The ethyl acetate solution of the organic-inorganic composite material containing AC33 / nanometer calcium hydroxide was painted from low to high in order from low to high on the mural fragments obtained from a tomb in Xi'an. The amount of painting for each mass fraction is until the mural residue no longer absorbs the solution. The interval between brushing from one mass fraction solution to another mass fraction solution is subject to the evaporation of the ethyl acetate solution.
[0023] Tes...
Embodiment 2
[0026] Weigh the commercially available AC33 solid and nano-calcium hydroxide powder and mix to make the mass ratio 4:1. The preparation of nano-calcium hydroxide refers to our patent: Chinese patent, patent number, 201711361358.7. Dissolving the mixture of AC33 solid and nano calcium hydroxide powder in ethyl acetate solution to prepare the mass fraction of 1%, 3%, 5%, 7% to prepare an organic-inorganic composite material containing AC33 / nano calcium hydroxide.
[0027] The ethyl acetate solution of the organic-inorganic composite material containing AC33 / nanometer calcium hydroxide was painted from low to high in order from low to high on the mural fragments obtained from a tomb in Xi'an. The amount of painting for each mass fraction is until the mural residue no longer absorbs the solution. The interval between brushing from one mass fraction solution to another mass fraction solution is subject to the evaporation of the ethyl acetate solution.
[0028] Test Results:
[0...
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