A kind of silicone button and preparation method thereof
A button and silicone technology, applied in the field of silicone buttons and their preparation, can solve problems such as paint stripping, low surface energy of silicone buttons, and difficulty in silk screen printing, so as to improve the lubrication effect, solve difficult silk screen or paint removal, and reduce the amount of chitosan Effect
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[0031] The preparation steps of above-mentioned embodiment 1-3 and comparative example 1-4 are as follows:
[0032] Step 1. Weigh the silicone rubber raw rubber according to the ratio in Table 1, put the silicone rubber raw rubber in an internal mixer and knead for 8 minutes, control the mixing temperature at 45-47°C, and control the workshop temperature at 22-24°C;
[0033] Step 2, weigh vulcanizing agent, release agent, hydrotalcite, chitosan, color paste, catalyst according to the ratio in Table 1, then add vulcanizing agent, release agent, hydrotalcite, chitosan to the silicone rubber mixing , color paste, and catalyst for secondary mixing, mixing for 15 minutes, the temperature of the rubber mixing is controlled at 45-47°C, and the temperature of the workshop is controlled at 22-24°C to prepare the mixed rubber;
[0034] Step 3. Put the mixed rubber obtained in Step 2 into the key mold for vulcanization. The temperature of the mold is controlled at 180-185° C., the moldin...
Embodiment 4
[0040] Step 1. Weigh 150 parts of silicone rubber raw rubber, put the silicone rubber raw rubber in an internal mixer and mix for 8 minutes, control the mixing temperature at 45-47°C, and control the workshop temperature at 22-24°C;
[0041] Step 2: Add 0.3 part of vulcanizing agent, 0.2 part of release agent, 0.15 part of hydrotalcite, 0.05 part of chitosan, 10 parts of color paste, 0.1 part of catalyst to the silicone rubber mixing, and carry out secondary mixing for 15 minutes. The rubber mixing temperature is controlled at 45-47°C, and the workshop temperature is controlled at 22-24°C to prepare the mixed rubber;
[0042] Step 3. Mix the rubber compound obtained in step 2 and 0.15 parts of carbon fiber treated with ortho-dibutyl ester surface activation and put it into a key mold for vulcanization. The mold temperature is controlled at 180-185°C, the molding time is 56-58S, and vulcanization is formed. Get the silicone button. Among them, the activation treatment process ...
Embodiment 5
[0044] Step 1. Weigh 150 parts of silicone rubber raw rubber, put the silicone rubber raw rubber in an internal mixer and mix for 8 minutes, control the mixing temperature at 45-47°C, and control the workshop temperature at 22-24°C;
[0045] Step 2: Add 0.3 part of vulcanizing agent, 0.2 part of release agent, 0.15 part of hydrotalcite, 0.05 part of chitosan, 10 parts of color paste, 0.1 part of catalyst to the silicone rubber mixing, and carry out secondary mixing for 15 minutes. The rubber mixing temperature is controlled at 45-47°C, and the workshop temperature is controlled at 22-24°C to prepare the mixed rubber;
[0046] Step 3: Mix the compounded rubber obtained in Step 2 and 0.15 parts of carbon fiber into the key mold for vulcanization. The mold temperature is controlled at 180-185°C, the molding time is 87-90 seconds, and vulcanization is formed to obtain the silicone key.
[0047] The silicone rubber keys of Example 3, Example 4 and Example 5 were tested for hardness...
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