Platycladus orientalis extract-containing composition as well as preparation method and application thereof
A technology of extracts and compositions, applied in the field of compositions containing thuja arborvitae extract, can solve the problems of waste of resources, low utilization rate of functional components of thuja arborvitae leaves, etc., and achieve the effect of stable system and high product safety
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Embodiment 1
[0076] (1) Crushing the hay of Arborvitae leaves, adding 10 times of 1,3-propanediol, extracting at 50°C for 3 hours at low temperature, and filtering to obtain polyol extract A, which is the fat-soluble component of Arborvitae leaves;
[0077] (2) Continue to add 40 times of 60% ethanol to the filter residue obtained in the above steps, heat and extract at 70°C for 2 hours, and filter to obtain ethanol extract B;
[0078] (3) Continue to add 40 times of pure water to the filter residue obtained in the above steps, heat-preserve and extract at 70°C for 3 hours, and filter to obtain water extract C;
[0079] (4) Concentrate the ethanol extract B obtained in step (2) under reduced pressure, concentrate to no ethanol, and combine it with the water extract C obtained in step (3) to obtain feed liquid D;
[0080] (5) Carry out column adsorption and decolorization of material liquid D (macroporous adsorption resin model D101), adsorption flow rate: 1BV / h, after the adsorption is com...
Embodiment 2
[0083] (1) Crushing the hay of Arborvitae leaves, adding 40 times of 1,3-butanediol, extracting at 40°C for 5 hours at low temperature, and filtering to obtain polyol extract A, which is the fat-soluble component of Arborvitae leaves;
[0084] (2) Continue to add 30 times of 80% ethanol to the filter residue obtained in the above steps, heat and extract at 60°C for 3 hours, and filter to obtain ethanol extract B;
[0085] (3) Continue to add 10 times of pure water to the filter residue obtained in the above steps, heat-preserve and extract at 90°C for 1 hour, and filter to obtain water extract C;
[0086] (4) Concentrate the ethanol extract B obtained in step (2) under reduced pressure, concentrate to no ethanol, and combine it with the water extract C obtained in step (3) to obtain feed liquid D;
[0087] (5) Carry out column adsorption and decolorization of material liquid D (macroporous adsorption resin model D101), adsorption flow rate: 3BV / h, after the adsorption is compl...
Embodiment 3
[0090] (1) Crushing the hay of Arborvitae leaves, adding 25 times of 1,3-propanediol, extracting at 30°C for 1 hour at low temperature, and filtering to obtain polyol extract A, which is the fat-soluble component of Arborvitae leaves;
[0091] (2) Continue to add 10 times of 95% ethanol to the filter residue obtained in the above steps, heat and extract at 40°C for 1 hour, and filter to obtain ethanol extract B;
[0092] (3) Continue to add 30 times of pure water to the filter residue obtained in the above steps, heat-preserve and extract at 80°C for 2 hours, and filter to obtain water extract C;
[0093] (4) Concentrate the ethanol extract B obtained in step (2) under reduced pressure, concentrate to no ethanol, and combine it with the water extract C obtained in step (3) to obtain feed liquid D;
[0094] (5) Carry out column adsorption and decolorization of material liquid D (macroporous adsorption resin model AB-8), adsorption flow rate: 2BV / h, after the adsorption is compl...
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