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A kind of operation method of thermal phosphorus production process

An operation method and process technology, which is applied in the field of thermal phosphorus production process, can solve problems such as poor production process parameters, low output and phosphorus yield, and difficult operation of electrodes, so as to reduce enterprise investment, ensure sustainability, and eliminate The effect of electrode deflection and fracture

Active Publication Date: 2021-11-23
孙志立
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The invention provides an operation method of a thermal phosphorus production process to solve the problems caused by the difficulty in leveling the electrodes and poor production process parameters during the production of large and medium-sized yellow phosphorus electric furnaces with three or more electrodes in the current three-phase process. Accidents such as furnace wall and furnace bottom burn-through, while solving the problems of high consumption, low output and phosphorus yield in production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

experiment example 1

[0043] In November 2016, a 30MW×3 large-scale phosphorus electric furnace of a Yunnan company used the operation method of the thermal phosphorus production process of the present invention to conduct a production test experiment for half a month, and produced 1205t of yellow phosphorus products, which was the same as the same period of production using the traditional operation method. Compared with the increased output of 215t, the production efficiency has been greatly improved, and the sublimation power consumption per unit product is 13256KWh / t.P 4 , 635KWh / t.P decreased compared with the same period when the traditional operation method was used for production 4 , if the operation method of a thermal phosphorus production process of the present invention is adopted for annual production, a large amount of energy consumption can be saved, and the growth cost of the enterprise can be reduced.

experiment example 2

[0045] From January to December 2017, the 25000KVA multi-electrode 2 of a company in Guizhou # The phosphorus production electric furnace adopts the operation method of the thermal phosphorus production process of the present invention, the daily output is generally about 35.5t, the highest is 45.53t, the monthly output is generally above 1000t, and the power consumption is lower than 13015KWh / t.P 4 , and the phosphorus furnace failure rate is low in the production process, the annual shutdown time is greatly reduced compared with the 25000KVA multi-electrode phosphorus electric furnace controlled by the general traditional operation method, and the energy consumption per unit product is lower than GB 21345-2015 "Energy per unit product of yellow phosphorus Consumption quota", which greatly reduces the maintenance cost, further reduces the production cost of the enterprise, and improves the profit of the enterprise.

experiment example 3

[0047] From March to December 2017, a company in Sichuan 25000KVA multi-electrode 2 # Phosphorus production electric furnace adopts the operation method of the thermal phosphorus production process of the present invention to start the original operation, and the sublimation power consumption during the trial production period (3-5 months) is 14515.85KWh / t.P 4 ; From June to September, sublimation power consumption is 13352.27KWh / t.P 4 , Sublimation power consumption from October to December is 13005.05KWh / t.P 4 , the annual average sublimation power consumption is 13200KWh / t.P 4 Below (output 9400t), electrode consumption is only 10.95kg / t.P 4 , The unit product energy consumption and electrode consumption are less, breaking and exceeding the best level in the history of the plant during the same period.

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Abstract

The invention discloses an operation method of a thermal phosphorus production process, which includes the following steps: (1) firstly use an electrode holder and a hydraulic lifting system to basically adjust and balance the position of the electrodes, and check the current of each electrode according to the ammeter and voltmeter; , voltage size is observed; (2) carry out comprehensive analysis and processing according to the observation result of step (1) and other process parameters of the phosphorus furnace, so that the position of each electrode, ammeter and voltmeter display numbers are basically consistent; (3) according to the furnace condition and process parameters, timely lift the electrodes, and repeat step (2) to coordinate and balance each electrode after lifting the active electrodes. The operation method of the thermal phosphorus production process provided by the present invention overcomes the defects of the traditional operation method, and optimizes the overall process parameters and operation indicators of the large and medium-sized multi-electrode phosphorus production electric furnace using three phases or more, so as to achieve energy saving and environmental protection , High-quality and high-yield, reduce the production cost of the enterprise, and prolong the service life of the phosphorus furnace.

Description

technical field [0001] The invention relates to the technical field of yellow phosphorus production, in particular to an operation method of a thermal phosphorus production process. Background technique [0002] The production process of thermal yellow phosphorus is between metallurgy and chemical industry. Both the basic principle, experience and the operation and control of electric furnace production equipment have distinctive characteristics. , full and excellent" play a very important role. [0003] The control of electrodes and process parameters is particularly important in the production process, and its adjustment effect directly affects the energy consumption of yellow phosphorus products and the quality of yellow phosphorus. During production, there is an electrode molten pool under each electrode in the yellow phosphorus electric furnace. At this time, if the electrode ends are in a horizontal plane (that is, the electrode position is balanced), all the electrod...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B25/027
CPCC01B25/027Y02P20/10
Inventor 孙志立姚之琦黄平张洪兵尹品云
Owner 孙志立
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