Rare earth composite stabilizing agent used for PVC and preparation method thereof
A rare earth composite and stabilizer technology, applied in the field of PVC stabilizers, can solve problems such as lack of competitiveness, unproven light stability, and reduce manufacturing costs, so as to achieve reduced usage, good long-term thermal stability, and responsiveness The effect of mild conditions
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[0027] Preparation of lanthanum p-toluate
[0028] (1) Take 20g of lanthanum chloride and place it in a beaker, then add 100ml of dehydrated ethanol solution to dissolve it, and configure it into a 0.20g / ml dehydrated ethanol solution;
[0029] (2) Put 25 g of p-toluic acid in a beaker, add 500 ml of absolute ethanol to dissolve it, place the beaker in a constant temperature water bath, heat and stir, and prepare an absolute ethanol solution with a mass of 0.05 g / ml. Then slowly add the solution prepared in the above system, the reaction temperature is 60°C, and stir for 45 minutes;
[0030] (3) Use a peristaltic pump to add 250 ml of sodium hydroxide ethanol solution with a molar concentration of 2 mol / L, and add in 60 minutes to make the pH of the solution 6.5, then stir at constant temperature for 1 hour. Let it stand for 12 hours, filter, wash with absolute ethanol, water, and absolute ethanol in sequence, and dry at 62°C to obtain lanthanum p-toluate.
[0031] Preparati...
Embodiment 1
[0040]40g of lanthanum p-toluate and 160g of calcium stearate were put into a high-speed mixer and mixed for 4 minutes to obtain a mixed stabilizer.
Embodiment 2
[0042] Put 80g of lanthanum p-toluate and 120g of pentaerythritol into a high-speed mixer and mix for 3 minutes to obtain a mixed stabilizer.
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